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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088284
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ' Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Tetracosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.50 2.88 ug/1 244993 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 91 2 Heptadecane 240 C17H36 000629-78-7 91^ 3 Tricosane 324 C23H48 000638-67-5 91/ 4 Triacontane ____________________ 422 C30H62 000638-68-6 91' Abundance Scan 3318 (35.498 min): 23322.D (-) m/z 56795 100.00% 57 A 71 43 85 5000

35.20 35.40 35.60 35.80 253 m/z 71710 76.54% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #73543: Tetracosane 43 57 71

5000 85 35.20 35.40 35.60 35.80 99 m/z 43.00 70.90% 1 I ll 155169183197 294 338 ITI ■ /'i. II r,, I I, I' " ' I " " I' '' ' I '' '' I ' ’ ' ■ I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 7 71 85 35.20 35.40 35.60 35.80 5000 m/ z 85.05 54.22% 99

rn/z-> '' I'' 40 60 ..... ...y..., 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #46165: Tricosane 4 3 57 35.20 35.40 35.60 35.80 m/z 41.00 23.51% 71 553 85

TT-p-r J. ^113127 155169183197211 I"'' ' I'''' I'''' I'''' I''''' I I'''' I 253 297 324 I'''' I'''' 11''' I' I ' ' ' ' I ' ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

23322.D NP091101.M Mon Oct 15 10:26:19 2001 Page 15.

NYC-WTC_000088284

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NYC-WTC_000088284Source: NYC Law Department, mirrored locally

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