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GC/MS analysis report for sample AD22494, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22494 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086852–000086871

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086860
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Tetracosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

35.53 3.07 ug/1 288767 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

^1 Tetracosane 338 C24H50 000646-31-1 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Hexatriacontane_____________________ 507 C36H74 000630-06-8 91 Abundance Scan 3321 (35.526 min): 22494.D (-) m/z 57700 100.00% 57

43 71

553 85 7L ' ’ ' I ^.20 35.40 35.60 35.80 in/z 71.05 67.68% TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5)7 71

5000 85 7< 1 ' ‘ ' I 35.20 35.40 35.60 35,80 99 m/z 43.05 62.79% 1 294 338 I''''I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 43 7 71 ' ' I ' ' i\___ ' ’ ' I ’ ’ ' * I ' ' ' ' I 35.20 35.40 35.60 35.80 85 48.73% 5000- m/z85.00

'' I p-T'‘1-ryTTTYyTT-^Tp-VT-rYTT-TVp-riTyrT-TTp-TTTYTTTTJTT-I*TyTTTT^^ TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane V TY 57 35.20 35,40 35.60 35.80 71 m/z 55.00 22.66% 85 5000

99

134 ll 268 296 I'''' I'''' I' r T 7l/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

22494.D NP091101.M Wed Sep 26 15:26:54 2001 Page 7 NYC-WTC_000086860

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NYC-WTC_000086860Source: NYC Law Department, mirrored locally

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