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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089440
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\1\DATA\OCT3001\23836.D Vial: 16 Acq On : 31 Oct 2001 5:09 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Tetracosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.45 3.24 ug/1 411412 Perylene-dl2 37.15 Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Tetracosane 338 C24H50 000646-31-1 9]\ 2 Heptadecane 240 C17H36 000629-78-7 91\ 3 Octadecane 254 C18H38 000593-45-3 91/ 4 Heneicosane ____________________ 296 C21H44 000629-94-7 9]/ Abundance Scan 3312 (35.446 min): 23836.D (-) .. ' m/z 57700 100700% 57

43 71 85 5000

nZz-> Abundance XU 40 60 .J ®®113 jJ J 411551^183197211225239253267 . I Fl iT| . iTi I n . I fl I iT I. r., i",,. I'l. .

80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543; Tetracosane 309 . I 11I.. 1, 1,1,. p I i-i 111'l 111 1111 I '

m/z ' I'" I ' ' ' ' I ' ' ' ' I ' ' ‘ 35.20 35.40 35.60 35.80 71716 A 69.99%

43 57 71

5000- 85 35.20 35.40 35.60 35.80 99 m/z 43705 65.65% I I ll 155169183197 338 294 mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 . 340 Abundance #32063; Heptadecane _ , 57 71 85 35.20 35.40 35.60 35.80 5000 mTz 85.00 55.26% 99 7 j.7T.T.y, 1??. ' I I ' r i I • n I I . . . . I . H I , . . . I I . - 240 I'''' I'''' I'' " I' " ' I'''' I —= 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 7“ - 35.20 ~ 35.40 ,35.60^35.80-^ -43- ~71 m/z 55760 27.33% 85 5000

-rq-TT ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35,20 35.40 35.60 35.80

23836.D NP103001.M Thu Nov 01 13:27:29 2001 Page 16/

NYC-WfC_000089446'*“

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NYC-WTC_000089440Source: NYC Law Department, mirrored locally

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