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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089439
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT3 001\23836.D Vial; 16 Acq On : 31 Oct 2001 5:09 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS- 2 09 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 15 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.56 3.13 ug/1 489410 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Q"ual

1 Hexatriacontane 000630-06-8\9^ 507 C36H74 2 Heneicosane 296 C21H44 000629-94-7 51 3 Heptadecane 240 C17H36 000629-78-7 91 4 Pentacosane____ 352 C25H52 _____ 000629-99-2 91 Abundance Scan 3215 (34.555 min): 23836. D (-) m/z SYTOO 100.00% 57

5000 85

4' 34.20 34.40 34'60 34.80 ' ' ' 295 323 380 ' I " " I " " I " " I " " I " '' I " m/z71710 69.70% Ti/z-> Abundance 40 60

57 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #74636: Hexatriacontane J 5000- 85 ' I ' ' ' ' i^' 1 ' pi ■ r I I I 34.20 34.40 34.60 34.80 m/z 43.05 64.69% i 'j69 J97....................................................................... n/^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane 57— -

85 34.20 34.40 34.60 34.80 5000 m/z85.05 49.05%

TiZz-> Abundance --- 268-296 I'''' I'''' I " ' 11' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #32063: Heptadecane I" " I" " I" " I'.

z4 — 34.20=^34:40 ^34.60-34.80------- •m-/z—4TT05- -23.60% 85 5000

113

•nZz-> X 40 60 80 100 120 140 160 180 200 2^ '24O 260 280 300 320 340 360 380 34.20 34.40 34 60 34 80

23836.D NP103001.M Thu Nov 01 13:27:27 2001 Page 15 .

NYC-WTC_000089439

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NYC-WTC_000089439Source: NYC Law Department, mirrored locally

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