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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089441
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT3 001\23836.D Vial; 16 Acq On ; 31 Oct 2001 5:09 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 17 Benzenamine, 3-phenoxy- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 35.61 0.50 ug/1 63524 Perylene-dl2 37.15

Hit# Of 5 Tentatzive ID MW MolForm . CAS# Qua!

1 Benzenamine, 3/phenoxy- 185 C12H11N0 003586-12-7 23 2 Naphthalene, -isothiocyanato- 185 C11H7NS 000551-06-4 9 . 3 IH-Isoindol^ -1,3(2H)-dione, 2-(2-pr 185 C11H7NO2 007223-50-9 9 4 Phenol, 4/(phenylamino)- 185 C12H11NO. 000122-37-2 9 Abundance 7 Scan 3330 (35.611 min): 23836. D (-) m/z 185.10 100.00% Ite

5000- 70 112 43

4-*UUl .............................. 203 253281 35.20 35,40 35,60 35.80 36,00 I I ' ' I ' ' ' • I ' ' ' ' I ' ' ' ' i ' ' ' ’ I ' ' ' ' I ' ' ■nTz 55.05 37.62% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69042: Benzenamine, 3-phenoxy- 11(5

156 5000 35.20 35'40' 35.60 35'80 os'oo 65 m/z 70.00 31.66% 77 32 130 168 II.......................................... TT-HS-r-p- n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #19180; ------- Naphthalene, ,--------- - 1-isothiocyanato- - . _ ..

153 35:20 35.40 35.60 35.80 36.00 5000 m/z 112.1030.55% 127 93 I ■, ........I;..........- .. I ’ ' ' ' I ’ ' • ' I ' I ' ' ' I I ' ' • ' I ' i n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #19179; 1 H-lsoindole-1,3(2H)-dione. 2-(2-propynyl)- --------- - ------ - ----- ig.--------------------------------- --- ^35.20" 35.40 35 60 35.80 36.00 m/z57.00' 29.44%“' ■■

5000 A _ .76 104 T57- 129

Tlfe-> 40 60 80 100 120 X 140 160 180 200 220 240 260 280 35.20 35.40 35.60 35.80 36.00

23836.D NP103001.M Thu Nov 01 13:27:31 2001 Page 17

NYC-WTC_000089441

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NYC-WTC_000089441Source: NYC Law Department, mirrored locally

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