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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088480
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NYC 9/11 Public Portal Document

Library Search Compound Report I Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D Vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 209 GALOS , Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209‘625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Hexadecane Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 38.36 0.90 ug/1 ' 85989 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 87__ 2 Triacontane 422 C30H62 000638-68-6 87 / 3 Heptadecane 240 C17H36 000629-78-7 87/ 4 Tritetracontane_________________________ 605 C43H88 007098-21-7 87 ' ^bundance Scan 3630 (38.362 min): 23272.D (-) m/z 57795 100.00% 57

552 85

38.00 38.20 38.40 38.60 m/z 71.00 69.81% n/z-> 40 60 80 100120140160180200220 240260280 300320340 360380 400420 Abundance #29267; Hexadecane 57

5000 85 38.00 38.20 38.40 38.60 “mTz 43705 77769% 1? 141 19G 226 I ‘' I" " I'"' I" ‘' I" " I TT/z-> 40 60 80 100120140160180200220 240260280 300320340360380400420 Abundance #55461: Triacontane 43 T 71 38.00 38.20 38.40 38.60 5000 m/z 85.05 44.73%

239 267 379 422 TTTpT I " " I I I H J H I I) I I I I I 11 I I |- I'I “'' r "' I" " I"' Tife-> 40 60 80 100120140160180200220 240260280 300320 340360380400420 '\bundance #32063: Heptadecane 57 38.00 38.20 38.40 38.60 “mTz 6^700 27773% 85 552

I 113 141 240 196 TTTjTTTTpT-rTyrTrTpTTTTrrTTyTTTTpTTrpTTTpT^^ ‘" I'' ■n/z-> 40 60 80 100120140160180200220 240260280 300320 340360380 400420 38.00 38.20 38.40 38.60

23272.D NP091101.M Mon Oct 15 09:42:28 2001 Page 18

NYC-WTC_000088480

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NYC-WTC_000088480Source: NYC Law Department, mirrored locally

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