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GC/MS analysis results for sample AD22578, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.

NYC-WTC_000087163–000087179

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087176
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report .Data File : C:\HPCHEM\l\DATA\SEP2801\22578.D Vial: 6 Acq On : 28 Sep 2001 5:19 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Tetratetracontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 33.72 0.42 ug/1 64905 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91^ 2 Heptacosane 380 C27H56 000593-49-7 91A 3 Docosane 310 C22H46 000629-97-0 83 / 4 Nonadecane 268 C19H40 000629-92-5 80 / Abundance Scan 3124 (33.717 min): 22578.D (-) m/z57700100.00% 57

5000 85

I, , Pj^/41i69 215 282 ^.40 33.60 33.80 34.00 in/z 71.10 71.30% ■nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 /Abundance #61068: Tetratetracontane 57

5000 85 33.40 33.60 33.80 34.00 in/z 4^705 63.55% |^r.^l\^69.1^.225 379407 590618 50 100 150 200 250 300 350 400 450 500 550 600 ^bundance #52248: Heptacosane 57

^3.40 33.60 33.80 34.00 5000 85 m/z 85.05 45.28%

380 ' I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Tnlz-> 50 100 150 200 250 300 350 400 460 600 660 600 Abundance #44318: Docosane 57 33.40 33.60 33.80 34.00 In/z 55.00 21.46% 85 5000

266 310 ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 33,40 33,60 33.80 34.00

22578.D NP091101.M Wed Oct 03 11:30:08 2001 Page 7 NYC-WTC_000087176

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NYC-WTC_000087176Source: NYC Law Department, mirrored locally

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