Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
NYC-WTC_000034213–000034226Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\28271.D Vial: 26 Acq On : 27 Nov 2001 1:21 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************************************** * * *** ******** ** * * * * Peak Number 6 1,171,3,5,7,7,7-Octamethyltetr Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
47.05 0.71 ug/1 90684 Perylene-dl2 37.11
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,3,5,7,7,7/0ctamethyltetrasilo 282 C8H2603Si4 000000-00-0 9 2 Pyridine, 3,5-dichloro- 147 C5H3C12N 002457-47-8 7 3 cis-2,3 -Methylenedioxy- .beta . -methy 207 C10H9NO4 000000-00-0 5 4 Pyrido[2yg-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 4 Abundance di Scan 4575 (47.046 min): 28271 .D ?) m/z 147.05 100.00%
.A | 147 221
5000 । 341 41 96 267 295 369 430 —+4—A44 — MMAAA 46.80 47.00 47.20 47.40 111 100 |I !r । 193 i ।| m/z 221.00 87.80%
A m/z-2__ 50 150 200 250 3(0 350 400 Abundance #39662:1,1,1,3,5,7,7,7-Octamethyltetrsriloxane 207
73 TT-j-n- 5000- 46.80 47.00 47.20 47.40 267 m/z 207.00 82.89%
mlz-> i 15 ----- 50 45 ।
100_._ AL 150 200 250 300 350 400 Mpow“Wwa- Abundance #8989: Pyridine, 3,5-dichloro- ( 147
46.80 47'00 47.20 47.40 ' 112 5000 i 50 m/z 340.90 46".77% 85
i m/z—>__ 50 100 150 200 250 300 350 400 Abundance #24525: cis-2,3-Methylenedioxy-.beta .-methyi- beta. -nitrost ' ■ i ' ■ ■ ■ I ‘ > I • ‘ 77 103 147 207 46.80 47.00 47.20 47.40 m/z 355.00 31.70% 51 5000 •
| j 1 L 179 I.................. . , । ■ ' l ■ ■ TIIT m/z-> 50 100 150 200 250 300 350 400 46.80 47.00 47.20 47.40
28271.D GCMS1126.M Wed Dec 05 13:15:00 2001 Page 6
NYC-WTC_000034225
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NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder