Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
NYC-WTC_000033765–000033779Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28159.D vial: 21 Acq On : 27 Nov 2001 6:15 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
41.54 2.53 ug/1 447190 Perylene-d12 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7- eptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 37 2 3,6-Dioxa-2,4, ,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 3 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 14 4 4H-Pyrido[l, -a]pyrimidine-3-carbox 221 C11H15N3O2 064399-29-7 14 Abundance Scan 3975 (41.539 min): 28159.D (-) m/z 73.00 100.00% 73 147 221 5000 281 355 T T T T T 429 41.20 41.40 41.60 41.80 191 I m/z-> 43 ,96 th TITTNTT.. T - ... 4 .. 327... mOonpnn m/z 40 60 80 100120140160180200220240260280300320340360380400420 401 1 147.00 72.69% ................. .................................... Abundance #56714:1,1.1.5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 5000 267 41.20 41.40 41.60 41.80 355 429 45 207 m/z 221.0563.13% _/ 1H lr “1 "T‘‘UI‘"‘1EETTT‘T‘T‘‘IT rr ।" " । . . TTTT m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 ""I 73 41.20 41.40 41.60 41.80 5000 m/z 281.00 27.82% 191 117 279 mpmmmmmmm mmle - mrmpa i, i pm me m mpmmmmpmm mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #72972:1,2-Benzenedicarboxylic acid, bis(trimethylsily!) e 147 41.20 41.'40 41.60 41.80 1 m/z 207.00 26.21% 73 5000
45 295
m/z—> ""'I 'I1' +ls.++ 193 221 I TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT ’ 40 60 80 100120140160180200220240260280300320340360380400420 ■ ■ i'11 n • ■ ■11 •11111 ■ ■' i 41.20 41.40 41.60 41.80
28159.D GCMS1126.M Wed Nov 28 11:15:58 2001 Page 5
NYC-WTC_000033776
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NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034213
Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder