Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
NYC-WTC_000034213–000034226Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV2601\28271.D Vial: 26 Acq On : 27 Nov 2001 1:21 pm Operator: 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3,6-Dioxa-2,4,5,7 - tetrasilaoct Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
39.59 0.84 ug/1 108140 Perylene-d12 37.11
Hit# Of 5 Tentative/ID MW MolForm CAS# Qual
1 3,6-Dioxa-2;4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 28 2 1,3-Benzodioxole, /5- [3-acetaminopro 221 C12H15NO3 000000-00-0 27 3 Mercaptoacetic acid, bis (trimethyls 236 C8H2002SSi2 006398-62-5 17 4 3-1 s opr op oxy-1, L, 1,7,7,7- hexamethyl 576 C18H5207Si7 071579-69-6 17 Abundance ‘Scan 3763 (39,592 min): 2827Tb (-) .................... m/z 1 , 73.00 100.00% 73
147 221 5000
281 355 I 39.20 39.40 39.60 39.80 40.00 41_ 96__________________________ 327 1 ____ _______ ________ 401 429 i_H+ TTuTgn m ’ TTTTTTITTTTTTr l TTCTTTTTITTTi ■ rf.. .. । . ‘ I m/z 146.95 67.47% m/z—>__ 40 60 80 1001201 40 16018 0 200 220 240 26 0 280 300 3203403-30380 400 420 __ Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2:2.4,4,5,5,7,7- 147 221
73 5000 ‘ 39.20 39.40 39.60 39.80 40.00 191 52.58% 117 279 L -H 40' 60' 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 m/z—> Abundance #27829:1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221 * * j » ' 135 162 39.20 39.40 39.60 39.80 40.00 73 m/z 207.00 32.87% 5000 | AN/WAmAW 104 i 49 n ITfrT — 4 ! . TTTTTT] „ 192. 3 J T TTTTT ‘IEIIUEEU‘E"I"7TT TTUUTTEFTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300320 340 360 380 400 420 Abundance #30949: Mercaptoacetic acid, bis(trimet iyisilyl)- 73 39.20 39.40 39.60 39.80 40.00 147 23.67% m/z 355.05
5000
m/z-> 45 104 TTTTT 1 193 221
40 60 80'100120140160 780 200 220 2482807280 300 320 310 360 383 400 420 "' J T I T‘"OT , T 39.20 39.40 39.60 39.80 40.00
28271.D GCMS1126.M Wed Dec 05 13:14:54 2001 Page 3
NYC-WTC_000034222
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NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder