Laboratory report detailing GCMS analysis of sample AD28271 conducted on December 6, 2001.
NYC-WTC_000034213–000034226Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\28271.D Vial : 26 Acq On : 27 Nov 2001 1:21 pm Operator : 209 GALOS Sample : 11/21 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS 7 5 K . L ********************************************************************* Peak Number 4 3,6-Dioxa-2,4,5, 7-tetrasilacct Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 41.53 1.28 ug/1 163900 Perylene-d12 37.11 Hit# cf 5 Tentative ID MW MolForm CAS# Qual
1 3,G-Dioxa-2,4,5,7-t trasilaoctane, 294 C10H3002Si4 004342-25-0 32 2 3-Isopropoxy-l,1,1, , 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 3 Cyclopropanamine N-methyl-1-phenyl 147 C10H13N 056771-48-3 12 4 Pent anoic acid, [ (trimethylsilyl) 2 62 C11H2603Si2 055887-46-2 12 Abundance Scan 3974 (41.529 min): 28271. C (-) m/z / 73 147 221 5000 I
L 281 355 327, , 401-I 429 41.20 41.40 41.60 41.80 — ■' 44
miz—>______ 50I - 15 100 — 4 150 193 200 250 300 350 400 -150 50 □ 550 m/z 146.95 ................/ 77.30% Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2.2,4,4,5, 5,7,7- j 147 221
1 73 5000 41.20 41.40 41.60 41.80 191 m/z 221.05 64.66% 117 279
m/z—> 50 4 TT “ITT 100 150200 l 250 300 --------........................... — 350 400 450 500 550 Abundance #60503 3-isoprcpoxy-1,1,1,7,7,7-hexamethyi-3,5,5-tris(trim ! 73 / "A~ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ' i 41.20 41.40 41.60 41.80 5000' m/z 207.00 41.16% 147 i 221 WMMNAK 281 327 415 519 561 1 • I 1 1 1 1 TT. ' Ti ■ ~T ■ —— TT ' i 1 ■ miz->50 100 150 200 250 300 350 400 450 5(J 550 Abundance #9103: Cyclopropanamine, N-methyl-1 -phenyl- 147 41.20 41.40 41.60 41.80 m/z 354.95 22.39%
m/z—> 5000 :
. 42 j 1 92 1201 - Ir* PT. t j.. TTT.. tr । r. ii । । । । j i । । t । » : v -PPITT 1 TT j 50 100 150 200 250 300 350 ■’ 0 . 450 500 550 A 41.20 41,40 41.60 41.80
28271.D GCMS1126.M Wed Dec 05 13:14:56 2001 Page 4
NYC-WTC_000034223
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NYC-WTC_000034402
Laboratory report documenting GCMS analysis of sample AD28428 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034808
Laboratory analyst notes on GCMS scan results, recovery rates, and low pH conditions for sample AD28649.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034886
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034198
Laboratory report detailing GCMS analysis of sample AD28263 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034988
Laboratory report noting contamination from the TurboVap concentrator and recovery rates for sample AD28662.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033752
Analytical commentary for sample AD28159 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033834
Analytical commentary for sample AD28155 dated November 29, 2001, noting detection of bis(2-Ethylhexyl)phthalate and low recovery rates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033800
Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000034154
Single page of raw GCMS data or header information from samples tested in late November 2001.
Filed in the same folder
NYC-WTC_000034155
Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
Filed in the same folder
NYC-WTC_000034156
Instrument sequence log listing calibration standards and sample IDs processed between November 26 and 30, 2001.
Filed in the same folder
NYC-WTC_000034160
Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
Filed in the same folder
NYC-WTC_000034168
Laboratory report of GCMS calibration data for sample AD28263 conducted on November 26, 2001.
Filed in the same folder