GCMS analysis results for sample AD30601, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M: \ INSTRU~ 1\2 0 9\DATA\DEC2 701 \LBB. D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Chrysene-dl2 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.02 29.70 ug/1 6642890 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Chrysene-d12 2 1,4-Bis (6-methylpyridyl-3)-butane 240 C16H20N21 240 C18D12 001719-03-5 98 000000-00-0 47 >3 Nap htho [2,1-b:7,8-b'] difuran, 1,2,9 240 C16H1602! 068873-21-2 47 4 2,4 , 6,8,9-Pentathiatricyclo[3.3.1.1 240 C6H8S5 057274-63-2 43 Abundance Scan 3048 (33.022 min): LBB.D (-) m/z 240.15 100.00% 240

5000

106 120 32.60 32.80 33.00 33.20 33.40 0- r i 42 i52fi । 66 78 92 1'7 i l'| i l[ || 132 146156 170180 194 212222 1H m/z 236.15 24.78% mz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32068: Chrysene-d12 240

5000 32.60 32.80 33.00 33.20 33.40 m/z 239.1 21.21% 106 120 ------------ 156 212 ill 1 1 I ' 1 rr Tl i । । । । r i i] । i i-i m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32046; 1,4-Bis(6-methylpyridyl-3 jbutane 240 107 32.60 32.80 33.00 33.20 33.40 5000 m/z 241.15 18.64% 77 134 39 51 65 • ■ • । ■ ■ ■ ■ । । 92 * I • 1 • । 1 ■ ■ ■ i ■ ■ ■ ■ । l ■ 1 । 1 1 ‘ ■ । 1 * ■ ■ । ■ ■ • ■ । ■ ■ ■ ■ । ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32043: Naphtho[2,1-b:7,8-b’difuran, 1,2,9,10-tetrahydro-2 240 32.60 32.80 33.00 33.20 33.40 m/z 120.05 18.02% 5000 211 152 181 1?7 225 I , ,— , ,r m/z-> 40 60 80 100 120 140 160 180 200 220 240 32.60 32.80 33.00 33.20 33.40

LBB.D GCMS0103.M Thu Jan 10 13:58:58 2002 Page 6

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