Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
NYC-WTC_000017126–000017138Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzeneethanamine,. N-[(pentafl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
22.79 0.58 ug/1 281018 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 27 2 N-(Trifluoracetyl)-0,0’,0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 25 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Trisil ane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Abundance Scan 1933 (22.786 mln): LBB.D (-) m/z 73.0,0 100.00% 73
5000 147 355 ! 221 281 i 45 117 191, 191 1 251. | 327 [ 401 22.40 22.60 22.80 23.00 23.20 — T r r j 1"I TI’ i > -'i । । । i t f । •. . . । । । i । । . m/z 147.00 27.33% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-((pentafluorophenyl)methyleneJ 73 355
5000 22.40 22.60 22.80 23.00 23.20 m/z 355.05 22.65% 45 . L, I 1 'I ' 1 t i । r-n-. | 208 251 281 । 386 458 548 . 1**** i‘ • ■ ■ i ■ ■ ' ■ i ■ • ■ • i • 1 ■ • i ' • m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53807: N-(Trifluoracetyl)-0,0’.O"tris(trimethylsilyl)epin 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.54%
45 140 184 281 I 480 PBTus ■11 ‘■■ ir'111 • ■ • ■ । • ■ ■ ■ । ‘ • ■11' * • ■ । ■ ■ ■ ■ i ■ • ■ 1 i ■ • ' 1 i ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5.5-tris(trim 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 13.34% 5000 147 221 281 327 415 519 561 / । 1 1 -ndn/n/n/nnn—n/mnBnn—mnnnnin F— IIIIIIt’i m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
LBB.D GCMS0103.M Thu Jan 10 13:58:53 2002 Page 5
NYC-WTC_000017136
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NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder
NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
Filed in the same folder