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GCMS analysis results for sample AD30607, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.

NYC-WTC_000017171–000017191

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017184
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~l\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr.: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************** * * ********************************* Peak Number 7 N-(Trifluoroacetyl)-N, 0,0',O'1 Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.79 1.81 ug/1 758689 Phenanthrene-dl0 24.99 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 N- (Trifluoroacetyl)-N,O,O’,0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 35 2 N-(Trifluoracetyl)-0,0’,0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 35 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3S13 055429-13-5 32 4 Benzoic cid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 28 Abundance Scan 1933 (22.792 min): 30607.D (-) m/ z 73.00 100.00% 73

5000 147 355 221 281 45 117 191, | 251 [ 327 401 22.40 22.60 22.80 23.00 23.20 ■ th50+ -1 TTPT 1*TTe 1 4 , L ■___________________________________ * • ' | * • < 1 | * ' * * | * ' * * | ‘ * m/z 355.05 27.89% mlz-> 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O )O’,O''-tetrakis(trimethylsl 73

355 5000 22.40 22.60 22.80 23.00 23.20 m/z 147.00 27.45% 45

m/z-> —4 100 50 147 193 150 ~ 200 267 250 300 ‘ 350 400 ‘ 450 ' 500 ’ 550 ' 538

Abundance #58807: N-(Trifluoracetyl)-0,0‘.O"-tris(trimethylsilyl )epin 73 355 l ‘ 1 1l •7**4* 1 * * 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.80% 45 140 184 281 480 ................ •1***t* ' 11 i • miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ................. ..... ‘73 355 2240 22.60 22.80 23.00 23.20 m/z 281.00 15.49% 5000

45 208 251 281 386 458 548 ■ • i ■ • ■ • I 1 ' 1 1 I 1 fl‘anmida)muai 9——1——B1—=9—m2TT m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30607.D GCMS0103.M Thu Jan 10 14:56:04 2002 Page 7

NYC-WTC_000017184

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NYC-WTC_000017184Source: NYC Law Department, mirrored locally

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