NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~l\209\DATA\DEC2701\30607.D Vial: 33
Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Mise Multiplr.: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
********************************** * * *********************************
Peak Number 7 N-(Trifluoroacetyl)-N, 0,0',O'1 Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.79 1.81 ug/1 758689 Phenanthrene-dl0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 N- (Trifluoroacetyl)-N,O,O’,0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 35
2 N-(Trifluoracetyl)-0,0’,0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 35
3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3S13 055429-13-5 32
4 Benzoic cid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 28
Abundance Scan 1933 (22.792 min): 30607.D (-) m/ z 73.00 100.00%
73
5000
147 355
221 281
45 117 191, | 251 [ 327 401 22.40 22.60 22.80 23.00 23.20
■ th50+ -1 TTPT 1*TTe 1 4 , L ■___________________________________
* • ' | * • < 1 | * ' * * | * ' * * | ‘ * m/z 355.05 27.89%
mlz-> 100 150 200 250 300 350 400 450 500 550
Abundance #60162: N-(Trifluoroacetyl)-N,O )O’,O''-tetrakis(trimethylsl
73
355
5000
22.40 22.60 22.80 23.00 23.20
m/z 147.00 27.45%
45
m/z->
—4 100
50
147 193
150 ~ 200
267
250 300 ‘ 350 400 ‘ 450 ' 500 ’ 550 '
538
Abundance #58807: N-(Trifluoracetyl)-0,0‘.O"-tris(trimethylsilyl )epin
73
355 l ‘ 1 1l •7**4* 1 * *
22.40 22.60 22.80 23.00 23.20
5000 m/z 221.05 18.80%
45
140 184 281 480 ................
•1***t* ' 11 i •
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ................. .....
‘73 355 2240 22.60 22.80 23.00 23.20
m/z 281.00 15.49%
5000
45
208 251 281 386 458 548
■ • i ■ • ■ • I 1 ' 1 1 I 1 fl‘anmida)muai 9——1——B1—=9—m2TT
m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30607.D GCMS0103.M Thu Jan 10 14:56:04 2002 Page 7
NYC-WTC_000017184
OCR can misread numbers and units. Confirm readings against the page image before using them.