GCMS analysis results for sample AD30607, Jan 2002

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Data File : M:\lNSTRU~l\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.05 0.82 ug/1 343901 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 enzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 97 4-Methoxyphenylacetic acid ethyl es 194 C11H14O3 014062-18-1 43 3 Benzenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43

’.- 4 1-CyclopentXne-l-propanoic acid, .b 168 C10H16O2 061833-30-5 42 Abundance Scan 1743 (21.048 min): 30607.D (-) m/z 120.95 100.00% 121

5000 149 138 194 20 65 93 166 ' 1 I ' 1 20.80 21.00 21.20 21.40 39 50 J 77 il riTm j 11 ■ 111 ■ ■ r 11 P’s , |-l'. i . | Hti [ ■ I ‘I |'i ■ ■ ■ ri 11 109 ,.. 158.4/11179—7 ‘ I‘* m/z 149.00 45.54% mfa-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 138 194 20.80 21.00 21.20 2140 65 93 166 m/z 194.0 28.09% 27

m/z-> I 111.. IJ. t • 11111.1». I. J. 11.1.. I > I. . ।. । iL 11111, । >.. > । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ।..... Ip I , ।।।. “1“ Abundance #21247; 4-Methoxyphenylacetic acid ethyl ester 121 ■ ' i ' • ‘ • i • ‘ 1 ‘ i 1 ‘ 0" 20.80 21.00 21.20 21.40 5000 m/z 137.9 25.03% 194

51 85 7891 106 148 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21262: Benzenepropanoic acid, 4-methoxy-, methyl ester ■ 1 i ' ■ ■ ■ l > UTYM? 1 121 20.80 21.00 21.20 21.40 m/z 64.9 19.02% 5000 194 134 111 < । | < 1111 > i > > । < < > 111 < ’ 1’14 . j »rrq 108 . —I uu10011199031 I. 151 163 —90BBBTTTTTTTTT A,A - 44 r “ ■ r " ■! “ I “ T T m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21,00 21.20 21.40

30607.D GCMS0103.M Thu Jan 10 14:55:59 2002 Page 6

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