GCMS analysis results for sample AD30633, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

21.05 0.93 ug/1 416437 Acenaphthene-dl0 20.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Benze: propanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43 3 1-Cyd opentene-1-propanoic acid. .b 168 C10H16O2 061833-30-5 42 4 Ethanone, 1-(4-ethoxyphenyl)- 164 C1OH1202: 001676-63-7 42 Abundance/” Scan 1743 (21.048 min): 30633.D (-) m/z 120.95 1 00.00% 121

149 5000 138 194 65 93 166 ' 1 i 1 1 1 1 r1 1 1'' 11111 !I 39 20.80 21.00 21.20 21.40

miz-> TIT --2,77854— 50 109 TTTTM “ । ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I h l 179 1,. *d*.., ।. ,T, ।. 11 .j .... 11 ................... " 50.14% Abundance #21260: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 ■ ■ i • • • > i • ■

138 20.80 21.00 21.20 21.40 194 65 93 166 m/z 194.05 30.15% 27 1 TWmmapT }’* +1* t . k । i M . j . . . » । » . » » । . ‘ I “ “ 11 • • * I ‘ * ’ ‘ I i■ ■■ ■ i“ “i • miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #21262; Benzenepropanoic acid, 4-methoxy- methyl ester 121 1 T ! > f I I I l mimmer 20.80 21.00 21.20 21.40 5000 m/z 137.95 28.10% 194 134 108 151 163 ’190011—0—m—0mTmuu911TnuuaTT i “ > > i ■ ■ ■ • i. • i, ।. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #14561:1-Cyclopentene-1-propanoic acid, .beta.-methyl-, me • • j ■ •

58 79 95 12!1 20.80 21.00 21.20 21.40 8000 m/z 64.95 19.95% 109 6000;

4000: 150

m/z—> 'lINniiiupn'iH' liuipiupi.ip • ‘ I ”' T’u 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 r. . I 168___________ ■ ■■ • i ■ • ■ > i1H1 r ■ ■ ■ i “ " i • • N *, P. , , , , (1 , , MM 20.80 21.00 21.20 21.40

30633.D GCMS0103.M Thu Jan 10 15:24:05 2002 Page 7

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