NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS analysis results for sample AD30633, Jan 2002
Machine-extracted title · confidence 95%Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
NYC-WTC_000017210–000017232Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\lNSTRU~l\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
20.28 5.14 ug/1 / 2300070 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H5207S17 071579-69-6 38 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 22 4 Phosphori acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 10 Abundance Scan 1659 (20.277 min): 30633.D (-) m/z 73.00 100.00% 73
5000 147 281 t i । ii i i j i i r I । j । । T । i » 327 20.00 20.20 20.40 20.60 45 191 221 251 1 1355 383/15 — II I 117 i»i -* zoT r* Pi , , 1fi* PiipiBi'I TAIFIUI i 111" * m/z 147.00 36.25% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3.5.5-tris(trim 73
J V 5000 147 20.00 20.20 20.40 20.60 221 281 m/z 281.0.0 35.14% 327 ..... 415....... 519 561 * » * । > ' » * i • * > > । » < * i i * i > , । i < miz-> 50 100 150 200 250 300350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1.1.5.5,5-hexamethy-3,3-bis[(trimet 73 147 281 20.00 20.20 20.40 20.60 5000 m/z 326.9,0 13.86% 369 i 1 207 249, | 338 [ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily • • J • * • • J l » • • IT » I » J l I 73 20.00 20.20 20.40 20.60 m/z 282.00 9.86% 327 5000 . 237 45
■ ■ i • ■ 147172 212?4— 1 I (1 i ________ r i ‘‘ ■ i • ■1 ■ । ■ ■ ■ ■ i ■'' ■ i • • --- m/z~> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30633.D GCMS0103.M Thu Jan 10 15:23:59 2002 Page 6
NYC-WTC_000017222
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NYC-WTC_000017222Source: NYC Law Department, mirrored locally
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Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
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Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
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