Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
NYC-WTC_000017144–000017156Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\lNSTRU~l\209\DATA\DEC2701\30601.D Vial: 29 Acq On : 28 Dec 2001 5:20 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
20.28 0.98 ug/1 516591 Acenaphthene-dl0 20.56
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 10 4 Phosphoric id, 2-(methoxyimino)-3 415 C13H34NO6PSi3 055319-85-2 9 Abundance Scan 1660 (20.280 min): 30601 .D (-) m/ z 73.00 100.00% 73
5000 147 281 327
m/z-> - 45 50 117 100 191 221 251 Pr 1 ' ■ ■ ri Piu T'~' 150 200 250 300 L 400 450 500 ‘ 550 m/z 147.00 350 383,415 20.00 20.20 20.40 20.60 36.99% Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tfm 73
) 5000 - 147 20.00 20.20 20.40 20.60 221 281 m/z 281.00 3 6.40% 327 415 519 561 ’ I’***I+*’I’*I* -' ■ i ' ■ ■ ■ i ■ • ■ ■ i ■ ’ • ■ i ‘ ■ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1,1 5.5.5-hexamethyl-3,3-bis[(trimet 73 147 • • l < • • • l V■ 1 i T 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 14.25% 389 207 249 | 338 I m/z-> 50 100 150 200’ 250 300 350 400 450 500 ‘ 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 10.19% 327 5000 237 45
m/z—> 147 I 172 212 ■ ■ i ' • ■ ■ i ■ ■ • ■ i ■ ■ • ■ i ‘ 50 100 150 200 24250 — ---------- 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30601.D GCMS0103.M Thu Jan 10 14:05:29 2002 Page 4
NYC-WTC_000017154
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NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017233
Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018923
GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018858
GCMS analysis report for sample AD30606 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017157
Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018870
GCMS analysis report for sample AD30485 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017770
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036931
GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder