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GCMS analysis results for sample AD30601, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.

NYC-WTC_000017144–000017156

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017155
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30601.D Vial: 29 Acq On : 28 Dec 2001 5:20 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzeneethanamine, N-[ (pentafl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.80 0.61 ug/1 / 298243 Phenanthrene-dl0 24.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethan tine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 Tri siloxane,. 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 25 4 N- (Trif luo: acetyl)-N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 22 Abundance Scan 1934 (22.795 min): 30601. D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 i 45 117 191. [ 249, [ 327 401 22.40 22.60 22.80 23.00 23.20 m/z-> er 50 , IPT । i r Pirir 11 i ih 11hi -------------- 100 150 200 250 300 350 400 450 500 550 m/z 355.05 28.80% Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 .4....... 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 26.71% 208 251 281 386 458 548 • • । • ■ • ■ । > i11111 ■ ■ 1 ■ । • t+t I ' ‘ ‘ * I ‘ ‘ ' I ' ' ‘ ' I ' ' r-1 l ■ > I T-J r i m/z-> 50 100 150 200 250300 350 400 450 500 550 Abundance #52459; Trisiloxane, 1,1.1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.79% 369 207 249, 338 miz-> 50 100 150 200 ’ 250 300 350 400 450 500 ' 550T Abundance #74239: Phenethylamine, N-methyi-.beta.,3,4-tris(trlmethyfs / T T 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 16.83% 5000 355 44 147 193 267294 -r-t-r । n j » > । 4 j » » I » 4 11 * I t [ i ri । j i 4 i Ix i—i—i । j m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30601.D GCMS0103.M Thu Jan 10 14:05:34 2002 Page 5

NYC-WTC_000017155

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NYC-WTC_000017155Source: NYC Law Department, mirrored locally

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