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GCMS analysis log for sample AD30603

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.

NYC-WTC_000017233–000017245

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017244
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NYC 9/11 Public Portal Document 7: Library Search Compound Report : Data File : M:\INSTRU~1\209\DATA\DEC2701\30603.D Vial: 31 Acq On : 28 Dec 2001 7:17 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS ISIS IIIS IO IOI IOI IIHS IOI III ITA I TIT IIIA IOI ISAS AA A Peak Number 5 Benzeneethanamine, N-[(pentafl Concentration Rank 4 R.T. EstCone Area Relative to ISTD R.T. 22.79 0.58 ug/l 305575 Phenanthrene-d10 24.98 Hit# of 5 Tengative ID MW MolForm cas# Qual 1 Benzeneethanayine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 46 2 N-(Trifluoragetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Trisiloxane,/1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3___003618-20-0 37 ‘Abundance ‘Scan 1833 (22.788 min): 30603.D () m/z 73.00 100.00 | 00 | 147 201 355 i 45 Me 401 22.40 22.60 22°80 23.00 23.20 \ Bd ta. m/z 355.05 25.71 iz > 50. 400 _150_ 200 250 300 _350 400 450 500 _550_ ‘Abundance. #74708; Benzenesthanamine, N-(pentafluaropheniyijmethyiene] . i 355 | i i 22:80. 22.60 22.80 23100 23.20 | Pe Zz 147.00 23.94 i 208 251,281 386458 548 > __ 80100 _150__200__ 250 300350400 450 500550. Abundance np ‘#58807: N4Trifluoracety)}-0.0.O"-tis(timethyisily/jepin 1 | od 22440 22160 2218023100 2320 | 5000: | m/z 221.0, 18.34% | Eo 140 184 281 480 i Speer baie 50100 150 200 250 300 350 400 450 500550. ‘Abundance: ‘#52459: Trisiloxane, 1,1,1,5,5,5hexamethyi-3, Sbis|(timet — | 47 2240 22.60 22.80 23.00 23.20 | on m/z 281.0 14,18 | 5000: | 369 i 207 249 338 = mz-> «50-100 150-200 250 300 350400450 500550. 2240 22.60 22.80 23.00 23.20 30603.D GCMS0103.M Thu Jan 10 15:01:54 2002 Page 5 NYC-WTC_000017244

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NYC-WTC_000017244Source: NYC Law Department, mirrored locally

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