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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02”

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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 dan 2002 12:45 pm Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JOSS SI ISIS ISDE ISS IIIS IOUS I ISTITUTO ISEI IOI IOC ITO IIT III Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.63 1.04 ug/L 393076 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Benzeneetha: jine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N-(Trifluop6acetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 3 N-(Triflyéracetyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 4 Benzoic/acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 37 FRburdance Scan ie CAB MTD ‘| m/z 73.00 100.008 | 1 | 5000: i 147 355 | 22 281 | 45 401 22.40 22.60 22.80 23.00 | as eee eto One [nz 147.00 23.49 mz 50 100 150 200 250 350.400 450 500 550 | (Abundance #74706: Benzeneethanamine, N-[(pentafiuorophenyi)methylene) " | ] 7 | 5000: i 22.40 22.60 22.80 23.00 | 6 m/z 355.0 20.23 | --208__251,281 3e6___ 458, 548 ee 50100 150 200 250 300 350 400 450 500 550 ndance “456326; N-{Trifuoroacetyi-O.0°.0"-trs(trimethytsily!)no i ~ | | | | =e ‘22:40 22.60 22160 23.00 | | 5000: | m/z 221.0) 16.42% | 45 | | 120147 193 265 tt 481 wperreprerecr rere > 50 100_ 150. 250300 350 400 450500 580_| Abundance #58807: N-(Trifluoracetyi)-O 0", 0*-tris(trimethyisily)epin | ‘22.40 22.60 22.80 23.00 | 355 m/z 281.00 11.90 . 5000: * 140 184 281 480 iniz—> 50100 150 200 250 300 350 400 450 500550 22.40 22.60 22.80 23.00 31019.D GCMS0103.M Thu Jan 10 16:01:43 2002 Page 6 NYC-WTC_000017567

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NYC-WTC_000017567Source: NYC Law Department, mirrored locally

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NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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