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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017568
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 dan 2002 12:45 pm Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. Se Teetrrrrrrr rrr errstererrerrrrrrrrrr llr l irri titi tt rrtr rrr rr rrr 6s Peak Number 7 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 26.74 0.43 ug/1 162562 Phenanthrene-d10 24.81 Hit# of 5 ‘Textative ID MW MolForm cas# Qual 1 Trisiloxane/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 45 2 1,1,1,5,7,4,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 27 3 3-Isopropéxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16 4 Mercaptofcetic acid, bis(trimethyls 236 C8H20028Si2- __006398-62-5 10 Fourier ‘Scan 2363 (26.737 min): 31019.0 ¢) m/z 73.00 100.00 | | if 5000. | 447 | me lL 355 "2640 26.60 2660.27.00 45 429 £ ae tL Hed AEE f01 reryee | tafe 147.00 32037 fmz-> _ 80100 150__200__ 250300 _350__400___450__500__ 580 ‘Abundance #52459; Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bisi(trimet % 1 147 | 1 oot | 5000. 26.40 26.60 26.80 27.00 360 m/z 281.00 19.32 207 249, = r— > 50 100__150 200 250 300 350 400 450 500 550 Belge FESPA TT 1 5.77 7 Hopiametiyes, + bsteimathyisioy t 73 i ! 147 26.40 26160 26.80 27.00 | 8000- 267 m/z 221.0} 16.93 \ 385420 | ee 207 | | | fmven> "50160" 150200250 900350400 450.500 550 | Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tis(trim | 26.40 26.60 26.80 27.00 i m/z 74.10 8.26 | wis asa 415 519561 iniz—> 50100 150 200-250 300-360 400 —-450_ 500 550__| 2640 26.60 26.80 27.00 31019.D GCMS0103.M Thu Jan 10 16:01:48 2002 . Page 7 NYC-WTC_000017568

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NYC-WTC_000017568Source: NYC Law Department, mirrored locally

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GCMS calibration results · Box DEP Box 16

NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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