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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017612
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Je IEEE EOFS IOI ISTE OFT OS IOI ISIC III I TOTTI IDI SATII III IOS II OA AI IA Peak Number 11 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10 R.T. | EstConc Area Relative to ISTD R.T. 31.56 0.58 ug/l 122259 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Trisiloxang/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 2 Butanoic Acid, 3-methyl-3-[(trimeth 262 C11H2603Si2 055124-90-8 23 3 Ethanegfoic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 23 _4 3-Isofropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 (Abundance ‘Scan 2669 (31.563 min): g1022.D () m/z 73.00 100.00¥% | 5000; 147 | ma 281 | a. 429 |_31.20 31.40 31.60 31.80 fa waite erBiebetBrmclenre Sactrtita tn m/z 147.00 38.43 Ini, "40.60. 80.100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400420 [Abundance #52469: Tisloxene, 1.1,1,5,5,5-hexamethyl-3,3-bis{(trimet | nn : | 281 5000 rd 31.20 31.40 31.60 31.80 | 360 m/z 221.0, 24.34 207 249 338 bes “40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 __| (Abundance B3CIST: Butsroic acd. Smetyre|metyisiyioryk,t | Ed 131 | 31:20 “3140_31,60_ 31.80 | 000: m/z 281.00 15.82 i aS yo os five» "4D 60 "20.100 120 140 160 160 200 220.240 260 280 300 320 340 360 380 400 420 indance #30580: Ethanedioic acid, bis(trimethyisilyl) ester i rr te |_31.20 31.40 31.60 31.80 | | m/z 355.0 10.61 5000- - 45 \ 190 219 > ‘40.60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 31.20 31.40 31.60 31.80 31022.D GCMS0103.M Thu Jan 10 16:07:50 2002 Page 11 NYC-WTC_000017612

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NYC-WTC_000017612Source: NYC Law Department, mirrored locally

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