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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017613
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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE IES IIS HOISI I IIE IOI SEI ISI I OI IOI IOI IIS III IO III AI II III A Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 8 R.T. | EstConc Area Relative to ISTD R.T. 32.93 0.77 ug/l 162715 Chrysene-d12 32.84 Hit# of 5 Tefitative ID MW MolForm cas# Qual 1 1-Monolipéleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopp6poxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 3 Ethayédioic acid, bis(trimethylsily 234 C8H1804si2 018294-04-7 32 4 Proganedioic acid, [(trimethylsilyl 336 C12H2805Si3___038165-93-4 25 ‘Abundat ‘Scan 3038 (32.931 min): 31022.D ¢) ~T m/z 73.00 100.008 j | 5000 17 | (224 43 .W7 401 t one 429 32.60_32.80_33.00_33.20 tp Biderarb pero | m/z 147.00 41.849 mz-> 50100150 200-250 300350400 «450500550 Abundance #58871: 1-Monolinoleoyiglycerol trimethylsilyi ether | . i _ 47 a | | j | 32.60 32.80 33.00 33.20 | p34 | 193 | | 281 m/z 221.05 23.85% | | 395 | | ie2 Pan ane 0” _.200__250__300__350__ 400 _ 450_500_ 850 (Abundance F50S0S; JlSopropory-1.7.1.7.7.-hexamethyl-3 5 5-ms (tem if 73 i 32.60 _32.80_33.00_33.20 | 5000) m/z 281.00 16.633 147 | | eee ma>___'80. 100.160 200250300 350400450 500550 ‘Abundance +#30880: Ethanedioic acid, bis(trimethyisily) ester errr i 147 32.60 _32.80_33.00_33.20 m/z 207,00 13.02% . 5000: 45 | 190 219 Se imiz—> 80100180200 250 300350 400450500 550 ‘32160 $280 33003320 31022.D GCMS0103.M Thu Jan 10 16:07:56 2002 Page 12 NYC-WTC_000017613

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NYC-WTC_000017613Source: NYC Law Department, mirrored locally

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