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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02”

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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 dan 2002 12:45 pm Operator: 209 GALOS Sample : goms scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peerererrrrrrrrrrerr et rrtrrrrtrrrrtrrtriririirt ii lili ltr Peak Number 8 1-Monolinoleoylglycerol trimet Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 32.93 0.57 ug/l 148199 = Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 1-Monolinolegy¥iglycerol trimethylsi 498 C27H5404Si2 054284-45-6 50 2 Ethanedioig/acid, bis(trimethylsily 234 C8H1804si2 018294-04-7 27 3 Mercaptogyvecinic acid, tris(trimeth 366 C13H3004SSi3 000000-00-0 16 4 Silanamjfe, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 12 ‘Rbundance ‘Scan 3038 (82.834 min): 31019. (-) m/z 73.00 100.00 \ ' 5000- “ar } 224 281 365 ! a as 119 491 429 32.60 32.80 33.00 33.20 i 1 m/z 147.00 49.10 miz> 60.100 150 200 280 300 350400450 ‘Abundance #58871: 1-Monoiinoleoyiglycerol trimethylsilyl ether ' i 207 | 147 mepeee Boog wu '32160_ 3280 33.00 33.20 1 ans 28 m/z 221.0, 31.14 i 395 a2 ae vz-> ____§0 100 _150___200 _260 _300__360 __400 _450 a i #71005" Ethanediois acid, Bis(trimethyisily!} ester if | ; 147 ‘32160 32.80 33.00 33.20 | sco: m/z 281.00 20.28: : 45 i 447 190 219 ep eee ine 30 100 150, 250" 300 350 400 450 ‘Abundance #50900: Mercaptosuccinic acid, tris([rimethyisilyl) ester ! J 32.60 _32.80_33.00_33.20 i m/z 355.05 15.57 ies te | 245 276 393 351 mz 50100150200 250 30035040050 32.60 32.80 33.00 33.20 31019.D GCMS0103.M Thu Jan 10 16:01:54 2002 Page 8 NYC-WTC_000017569

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NYC-WTC_000017569Source: NYC Law Department, mirrored locally

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NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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