DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 1-Monolinoleoylglycerol trimet Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

35.06 0.35 ug/1 138495 Chrysene-dl2 33.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 37 43-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 3270 (35.060 min): 30648.D (-) m/ z 72.9^ 10 0.00% 73

147 5000 221 J 281 43 ' i ■ ■ I’I’M’I* 191 I 327 355 190 L 401 "4 ___ 34.80 m/z 147.00 35.00 35.20 35.40 54.85% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 34.80 35.00 35.20 35.40 34 103 m/z 220.95 25.43% 281

m/z->50 h ‘ ■ 1 i .. . ...aka... ... . 100 150 200 250 300 350 400 450 Abundance ' ■ / GNlo/paep: . 1 : , ‘ : r

73

147 34.80 35.00 35.20 35.40 5000 m/z 281.0.0 17.82% 45 117 190 219 ’ ’I’’ IIIIIIIIIIIIIIII m/z-2 _ 50 100 150 200 250 300 350 400 450 Abundance #30949: Mercaptoacetic acid, bis(trimethylsily!)- AAAAAAAN 73 34.80 35.00 35.20 35.40 147 12.86% 5000 221 45

m/z--> -4 50 104 100 | 150 193 I 200 I , 250 300 350 400 450 34.80 35.00 35.20 35.40

30648.D GCMS0103.M Thu Feb 14 11:02:20 2002 Page 14

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