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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017611
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peeereserercrrrrerrrrerererr: srerrrrrtr rir r rrr irri iti rt iret t ttt ttt ttt) Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 9 R.T. EstConc Area Relative to ISTD RAT. 30.09 0.76 ug/l 161455 Chrysene-d12 32.84 Hit# of 5 Texttative ID MW MolForm CASH Qual 1 1-MonolingYeoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 1,1,1,5/7,7,7-Heptamethy1-3,3-bis(t 444 C13H4005Si6é 038147-00-1 38 3 Silangfine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 12 4 Beng6ic acid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 10 [Abundance ‘Scan 2729 (30.084 min): 31022.D (¢) m/z 73.00 100.00 i i Ca 147 | . Pr er "880.3090 2020 "30140 i Le ae of m/z 147.00 35.17 > BD 100150200 2503003504005 Roi #5887 1: 1-Monolinoléoyigiycerol trimethylsilyl ether . | | 5000. 147 a a hk | 29.80 30.00 30.20 30.40 ™ 103 | |, 7a m/z 221.05 20.93 | | 25 a2 | mz-> so 10015020050 30038040040. | (Abundance #50714: 1.1,1.8.7,7.7-Heptamethyl 3, 3-bisimethyisiiogyt i 73 | “7 "79160 30,00 "90.20 8040 | s000. 267 m/z 281.00 13.47% | 355 429 45) 2 | mz> 50100150200 250-300-350 400450 ‘Abundance: ‘#39564: Siianamine, N-[2,6-dimethyi-4-[(trimethylsiiy)}oxy] | | 29.80 30.00 30.20 30.40 i] m/z 355.0; 13.353 . | 209 | se00) 4s | asi] | 425 147 78 bois ‘0 100 180-200-250 800380400450 ~""zele0 30.00. 30.20 30:40. 31022.D GCMS0103.M Thu Jan 10 16:07:45 2002 Page 10 NYC-WTC_000017611

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NYC-WTC_000017611Source: NYC Law Department, mirrored locally

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