NYC 9/11 Public Portal Document
Library Search Compound Report
Data File M:\INSTRU~1\209\DATA\JAN0802\31023.D Vial: 25
Acq On 9 Jan 2002 1:44 pm Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 9 1-Monolinoleoyiglycerol trimet Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
28.50 0.41 ug/1 145928 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Monolinoleoyiglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 40
2 Benzoic acid; 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38
3 Trisiloxa:ne, 1,1,1,5,5,5-hexamethyl 384 C12H36O4S15 003555-47-3 32
4 3-Isopropioxy-1,1,1,7,7z7-hexamethyl 576 C18H5207Si7 071579-69-6 28
Abundance / Scan 2555 (28.503 mln): 31023.D {-) m/z 73.0.0 100.00%
73
5000
147
221 281 355
28.20 28.40 28.60 28.80
45
I
117 . , . 1911 [ .. 327, ,1 401 429
• T nit * IT m/z 147.00 34.00%
miz-s 50 100 150 200 250 300 350 400 450
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207 ......................................................
5000 147
28.20 28.40 28.60 28.80
34 103 m/z 355.05 19.70%
281
I
.............. ..............395
1 482
t-[—r-T—r—r
m/z-> 50 100 150 200 '250' 300 350 400 450
Abundance #73975: Benzoic acid, 2.4-bis[(trimethylsily!)oxy]- trimet
73
28.20 28.40 28.60 28.80
5000 355 m/z 221.05 19.33%
45 ;
i 133 193 223 281
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147 28.20 28.40 28.60 28.80
281
m/z 281.00 16.46%
5000
369
m/z-> 50 100 150
2 249
200250
[ 338 . ...........
300' ' ' '350 ' ' 400 ' ‘ 450' ‘
...... .............
28.20 28.40 28.60 28.80
31023.D GCMS0103.M Thu Jan 10 16:12:16 2002 Page 9
NYC-WTC_000017645
OCR can misread numbers and units. Confirm readings against the page image before using them.