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GCMS analysis results for sample AD31023, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017630–000017648

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File M:\lNSTRU~l\209\DATA\JAN0802\31023.D Vial: 25 Acq On 9 Jan 2002 1:44 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-1sopropoxy-1,1,1,7,7,7-hexam Concent rat ion Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.74 0.57 ug/1 > 201496 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# . Qual

1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 59 2 1-Monolinoleoylglyceroltrimethylsi 498 C27H54O4Si2 054284-45-6 36 3 1,1,1,5,7,/7, 7-Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 25 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 25 Abundance Scan 2363 (26.740 mln): 31023.D (-) m/z 73.00 100.00% 73

5000 147 ) 221 281 45 2640 26.60 26.80 27.00 * 117 । iji 1 i’i-i 11 -i f 1 . . 1914 -.249- .. 327/325, , 399 428 .. .... m/z 147.00 32.35% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 26.40 26.60 26*80 27.00 ' m/z 281.00 17.80% ... 50 327, । . . . . 415. .59 561 100 ' 1 150 ‘ 200 ' ' 250 ' 300 ' 350 ' ' 400 ' 450 ' ' 500 550 ' m/z-> Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 . ..................... 207 26.40 26.60 26.80 27.00 5000 147 m/z 221.C5 15.86% 34 103 281 395 482 m/z-> ■ ' i ■ ■ ' ■ i ' ■ ‘ ■ I ' 1 ■ ' i ■ ' • ■ i ■ ■ ' 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 ' I ' ' ' ' I ' 1 1 1 I 1 1 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5.7,7,7-Heptamethyl-313-bis(trimethylsiloxy)t 73 26.40 26.60 26.80 27.00 m/z 207.00 8.56% 147 5000 267 355 429 45 207

m/z—> 50 100 150 200 250 300 350 400 450 500 550 26.40 26.60 26.80 27.00

31023.D GCMS0103.M Thu Jan 10 16:12:10 2002 Page 8 NYC-WTC_000017644

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NYC-WTC_000017644Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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