NYC 9/11 Public Portal Document
Library Search Compound Report
Data File M:\lNSTRU~l\209\DATA\JAN0802\31023.D Vial: 25
Acq On 9 Jan 2002 1:44 pm Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 3-1sopropoxy-1,1,1,7,7,7-hexam Concent rat ion Rank 8
R.T. EstConc Area Relative to ISTD R.T.
26.74 0.57 ug/1 > 201496 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# . Qual
1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 59
2 1-Monolinoleoylglyceroltrimethylsi 498 C27H54O4Si2 054284-45-6 36
3 1,1,1,5,7,/7, 7-Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 25
4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 25
Abundance Scan 2363 (26.740 mln): 31023.D (-) m/z 73.00 100.00%
73
5000
147
)
221 281
45 2640 26.60 26.80 27.00 *
117
। iji 1 i’i-i 11 -i f 1 . . 1914 -.249- .. 327/325, , 399 428 .. .... m/z 147.00 32.35%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000
147 26.40 26.60 26*80 27.00 '
m/z 281.00 17.80%
...
50
327, । . . . . 415. .59 561
100 ' 1 150 ‘ 200 ' ' 250 ' 300 ' 350 ' ' 400 ' 450 ' ' 500 550 '
m/z->
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
. .....................
207 26.40 26.60 26.80 27.00
5000 147 m/z 221.C5 15.86%
34 103
281
395 482
m/z-> ■ ' i ■ ■ ' ■ i ' ■ ‘ ■ I ' 1 ■ ' i ■ ' • ■ i ■ ■ ' 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 ' I ' ' ' ' I ' 1 1 1 I 1 1
50 100 150 200 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5.7,7,7-Heptamethyl-313-bis(trimethylsiloxy)t
73 26.40 26.60 26.80 27.00
m/z 207.00 8.56%
147
5000 267
355 429
45 207
m/z—> 50 100 150 200 250 300 350 400 450 500 550 26.40 26.60 26.80 27.00
31023.D GCMS0103.M Thu Jan 10 16:12:10 2002 Page 8
NYC-WTC_000017644
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