GCMS analysis results for sample AD31023, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

NYC-WTC_000017630–000017648

Folder label: “GCMS X 12/20/01 A 1/9/02”

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NYC 9/11 Public Portal Document

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Data File M:\INSTRU~1\209\DATA\JAN0802\31023.D Vial: 25 Acq On 9 Jan 2002 1:44 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.64 1.31 ug/1 464700 Phenanthrene-dl0 24.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 N- (Trifluoroacetyl) -0,0' ,0"-tris (t 481 C19H34F3NO4Si3 000000-00-0 37 3 Benzeneet namine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 Abundance ” / Scan 1916 (22.636 min): 31023.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 281 355 401 - .... —PPP 22.40 22.60 22.80 23.00 45 117' 191, [ 2511 327 m/z-> iat 1 *I—gTI 400 450 500 * 550 rn/z 147.00 26.34% 50 100 150 200 250 300 350 Abundance #58807: N-(Trifiuoracetyl)-0,0',0"-tris(trimethylsllyl)epin 73 355 5000 ■ ■ i ■ ' 1 I 1 1 22.40 22.60 22.80 23.00 45 rn/z 355.0 22.77% I I, 140 184 281 480 ■ ■ । ■ ■ ■ ■ । ■ 4 m/z—>50 100 150 200 250 300 350 ' 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-0.0,0"-tris(trimethylsilyl)no 73 355 r1 1 1 f' ' i ' 1 1 ' I 1 1 22.40 22.60 22.80 23.00 5000 m/z 221.05 17.46%

45 J 1 120147 193 265 481 ■ ■i■'■■ i■■■■i■ ■■■i • ■ ■ ■ i ■ ■ ■ • i ' 1 1 ■ i‘ ■ 1 ' i ' ■ ■ ■ i ■ ' ' ' i ■ ■ ‘ ■ i ' ■ rn/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 22.40 22.60 22*80 23'00 m/z 281.00 14.05% 5000

m/z~> I. 50 208 251 281 386 I’ * ‘ I‘‘‘‘I‘4 II/’di 1*’’’I*’’I’’’*I***1**’1** 100 150 200 250 300 350 400 458 450 500 548 550 *P 22.40 22.60 22.80 23.00

31023.D GCMS0103.M Thu Jan 10 16:12:04 2002 Page 7

NYC-WTC_000017643

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NYC-WTC_000017643Source: NYC Law Department, mirrored locally

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