Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
NYC-WTC_000017171–000017191Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-1sopropoxy-1,1,1,7,7,7-hexam Concentrat ion Rank 9
R.T. EstConc Area Relative to ISTD R.T.
26.89 0.78 ug/1 327950 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 56 2 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 33 3 Mercaptoacetieacid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 28 4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 17 Abundance / Scan 2379 (26.887 min): 30607.D (-) m/z 73.0.0 100.00% 73
5000 147 221 281 ......... / y....... 26.60 26.80 27.00 27.20 1 45 117 1 ''1 ’ ' 1*1 I ein ■ .1214/.251 , 327,355 401 429 ..... m/z 147.00 31.33% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tfs(trim 73
5000 147 11 T 26.60 26.80 27.00 27.20 221 281 m/z 281.0,0 16.03% 327 415 519 561 V+18***3T+[ — I I I • L,» ,I J I » I I I I » » » » I I » m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane. 1.1,1,5.5,5-hexamethyl-3.3-bis[(trimet 73 147 281 26.60 26.80 27.00 27.20 5000 m/z 221.05 15.40% 369 j 207 249, 338 , 1 ' i ' 1 ■ • i ■ ■ • ■ i 1 ■ 1 • i ' ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30949: Mercaptoacetic add, bis(trimethylsily!)- 73 147 26.60 26.80 27.00 27.20 m/z 74.0.0 8.30% 5000 221
m/z-> 4 45
50 104 100 ' 150 193 | 200 250 300 ' ' 350 ‘ ‘ 400 ‘ ' 450 ' ' 500 ' ‘ 550 ' ...... / \ ...... 26.60 26.80 27.00 27.20
30607.D GCMS0103.M Thu Jan 10 14:56:09 2002 Page 8
NYC-WTC_000017185
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NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder