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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017206
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NYC 9/11 Public Portal Document ‘ Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eerertrerrrrrrerenfsttrerrrrrttrrertrrtrrrtt tri tt itr ttt rt r rier irr rls Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7 R.T. | EstConc Area Relative to ISTD RT. 26.89 0.48 ug/1 204536 §Phenanthrene-d10 24.99 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 56 2 Trisiloxang/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 40 3 Ethanediove acid, bis(trimethylsily 234 CeH1so4si2 018294-04-7 25 4 Butanoi¢ acid, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 17 sundance ‘Sean 2379 (26.688 min}: 30608.0 () m/z 72.95 100.00% i 147 | 221 2t 358 ‘26.60 26190 27:00 27:20 | ET Raa Raan AT aanaT eaprnal Lat eaart ane w/z 147.10 30.87% la> 50 100 __150__200__250__300__360.__400_450__600_560 Bounces #0503: Slaopropoxy-1,1,1,7,7,7-hexamebiy-3 5 -nis(tim | bad | 147 —""z6160 26/80 27/00 27°20 | | m/z 281.0, 16.15% | | ieee ad ais 519564 vz 50. 1 150 __200 250 300 350 400 450 500 550 Abundance ° ae “Trisiloxane, 1,1,1,5,5.5-hexamethyl-3,3-bis|(trimet | | 2st ~"aaeo eo 2 27) | 5000: i m/z 221.0, 14.97% | ! 369 | i 207249, 338__| jance #30580: Ethanedioic acid, bis(trimethyisily!) ester | i 47 26.60 _26.80_27.00_ 27.20 | m/z 74.00 7.62% | 5000: | 45 L 190 219 > 50 400150 200 250 300350 400 450 500 550. 26.60 _26.80 27.00 27.20 30608.D GCMS0103.M Thu Jan 10 15:08:27 2002 Page 8 NYC-WTC_000017206

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NYC-WTC_000017206Source: NYC Law Department, mirrored locally

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