NYC 9/11 Public Portal Document
‘ Library Search Compound Report
. Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32
Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Misc : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
eerertrerrrrrrerenfsttrerrrrrttrrertrrtrrrtt tri tt itr ttt rt r rier irr rls
Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7
R.T. | EstConc Area Relative to ISTD RT.
26.89 0.48 ug/1 204536 §Phenanthrene-d10 24.99
Hit# of 5 Tentative ID MW MolForm cas# Qual
1 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 56
2 Trisiloxang/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 40
3 Ethanediove acid, bis(trimethylsily 234 CeH1so4si2 018294-04-7 25
4 Butanoi¢ acid, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 17
sundance ‘Sean 2379 (26.688 min}: 30608.0 () m/z 72.95 100.00%
i 147
| 221 2t
358 ‘26.60 26190 27:00 27:20
| ET Raa Raan AT aanaT eaprnal Lat eaart ane w/z 147.10 30.87%
la> 50 100 __150__200__250__300__360.__400_450__600_560
Bounces #0503: Slaopropoxy-1,1,1,7,7,7-hexamebiy-3 5 -nis(tim
| bad | 147 —""z6160 26/80 27/00 27°20
| | m/z 281.0, 16.15%
| | ieee ad ais 519564
vz 50. 1 150 __200 250 300 350 400 450 500 550
Abundance ° ae “Trisiloxane, 1,1,1,5,5.5-hexamethyl-3,3-bis|(trimet |
| 2st ~"aaeo eo 2 27)
| 5000: i m/z 221.0, 14.97%
| ! 369
| i 207249, 338__|
jance #30580: Ethanedioic acid, bis(trimethyisily!) ester
| i 47 26.60 _26.80_27.00_ 27.20
| m/z 74.00 7.62%
| 5000:
| 45
L 190 219
> 50 400150 200 250 300350 400 450 500 550. 26.60 _26.80 27.00 27.20
30608.D GCMS0103.M Thu Jan 10 15:08:27 2002 Page 8
NYC-WTC_000017206
OCR can misread numbers and units. Confirm readings against the page image before using them.