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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017312
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document : Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acg on : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : . Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS GIS ISI IIIS IOI IOI ISI IIS I III SI III III I III I SAI I IIASA Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8 R.T. EstCone Area Relative to ISTD R.T. 26.89 1.44 ug/l 713331 Phenanthrene-d10 24.98 Hit# of 5 Teftative ID MW MolForm cAS# Qual 1 3-Isopropoyf-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 Trisiloxaye, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 1-Monolifoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 4 Ethanefloic acid, bis(trimethylsily 234 C8H1804Si2 __—_—i0.18294-04-7 32 (Abundance: ‘Scan 2379 (26.685 min): 30634,D (-) m/z 73.00 100.00! “47 | | a aie 355 | 26.60_26,80_27.00_27.20 i 45 ¥ | Tape Eb PR ha BT SOLE w/z 147.00 32.56 miz>_50___100__150___200_250___300__350__400__450 _500__560 | pesca #60503: S-Tsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tim | | | 5000: | | | 147 |__26.60_26.80_27.00_27.20 | [m/z 281.0 17.04! i 22% 2 4 61 397 415 519 561 za 50. 100 150 200 250 300 350 400 450 500 550 a iia een S059: TWisiloxane, 1,1,7,5,5,5-hexamsinyi-s,sbe (rimot b 7 147 : 28 26.60 _26.80_27.00_27.20 f 8000 | m/z 221.0 16.40) 207 49 Pl > 50. 1 150__200 _250__300 _350__400 450 500 550 Abundance #58671: 1-Monolinoleoyiglycerol trimethyisilyl ether 26.60 _26.80 27.00 _27.20 | m/z 74.00 8.73) | 5000. sar 707 | i a 103 281 395 ae > 50100 150 250 300360 400 450 500 550 26.60 26.80 27.00 27.20 30634.D GCMS0103.M Thu Jan 10 14:10:03 2002 Page 7 NYC-WTC_000017312

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NYC-WTC_000017312Source: NYC Law Department, mirrored locally

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