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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017313
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NYC 9/11 Public Portal Document ° Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc ® Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JASE IO ISIS IOI IOFIOSIIOIOSI ISI IOI ISI IOI IS IOI IOI OI IIIT AT III Peak Number 8 Benzoic acid, 2,4-bis[(trimeth Concentration Rank 9 R.T. _ EstCone Area Relative to ISTD R.T. 28.66 1.13 ug/l 563066 Phenanthrene-d10 24.98 Hit# of 5 Tentgtive ID MW MolForm cas# Qual 1 Benzoic acid, /2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 30 2 N-(Trifluorgécetyl)-0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 25 3 3-Isopropoyy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Trisiloxafe, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 ‘ourdancs, ‘Scan 2572 (28.657 min}: S0834.D (-) m/z 73.00 100.00 i i [ad 17 | | 221 ogy 355 | ~ 28.40 28.60 28.80 _29.00 327, 429 i 45 417, 494. 249. 401, m/z 147.00 36.78: ine 50100 150 200 250 300 350 400 450 500 550 Abundance 1 #73075. Benzale acid, 24-bis[(rimethylalyjoxy}, timet | a a | ca 28.40 28.60 28.80 29.00 | m/z 355.0 21.49 i 133,493 223281 pviz—> 30 100 150. 200 260 300 350 450500 550_ dance #58326: N-(Teifuoroacetyl)-O.0;O"-tristtrimetiylsilylino | i 355 28.40 26.60 28.80 29.00 | 8000. m/z 221.0 21.42 i 45 i 120147 193265 481 mulz—> 50. 400 __150_ _200 250 300 350 400 450 500 550. Roane #60503: 3-1sopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-ris(iim: | 28402860 28.80 29.00 i m/z 281.00 16.77 | sooo: “7 | | | | in ed tts 519 561 miz> ___50__100__150__200 250 _300_350__400__450_ 500 550 28.40 _28.60_28.80 29.00 _ 30634.D GCMS0103.M Thu Jan 10 14:10:08 2002 Page 8 NYC-WTC_000017313

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NYC-WTC_000017313Source: NYC Law Department, mirrored locally

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