NYC 9/11 Public Portal Document
* Library Search Compound Report
. Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28
Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Misc : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
PeVrererrrrrrrrerret st Serre rr rrrerrerr rrr irri trr itr r ttt terer rrr ross
Peak Number 9 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 6
R.T. EstCone Area Relative to ISTD RT.
30.25 1.58 ug/1 498525 Chrysene-d12 33.03
Hit# of 5 Tentatjve ID MW MolForm caAs# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 33
2 Benzoic acid, 4,4-bis[(trimethylsil 370 C16H30048i3 010586-16-0 27
3 3-IsopropoxyA1,1,1,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 10
4 Silanamine /N- [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 9
‘Roundance ‘Sean 2745 (30.245 miny: SOBS4.D () Z 73.00 100.00
i) 1200) 147
: at A i 30.00 _30.20_30.
H ry 428 x 1.40 _30.60
| Bombe inte hinge ie “tinh | m/z 147.00 36.91
ylz-> 40 60 _80_100 120 140 160 180 200 220 240 260 280 300 320 340 360 380.400 420
Abundance ? ‘#66714: 1,1,1,5,7,7,7-Heplamethy/-3,S-bis(timethyisliony}t
{
t 147,
joo | id 355, 429. |» 30100 "30.20 ‘30140 ‘30.60
i ae 207 | | m/z 221.0 20.13
i t 4
mvz—> 40 60 _80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420
Abundance ‘#73975; Benzoic acid, 2.4-bis[(trimathylsilyijoxy}-. timet
if 2
| |" poo aaz0_ sola uso
| 5000: 355 | m/z 355.0! 12.46
| 4s
j 133 493223 281
miz> "40 60 8D 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400.420
‘Abundance ‘#49645: 3-Isopropoxy-1,1,7,5,5,5-hexamethyl-3-(timethyisil
i 281 30.00 30.20 30.40 30.60
m/z , °
281.0) 12.39
| $000 207
339
193477 rn
imiz—>____ 40-60-80 +100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 30.00 30.20 30.40 30.60 "|
30634.D. GCMS0103.M Thu Jan 10 14:10:14 2002 Page 9
NYC-WTC_000017314
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