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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017314
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NYC 9/11 Public Portal Document * Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L PeVrererrrrrrrrerret st Serre rr rrrerrerr rrr irri trr itr r ttt terer rrr ross Peak Number 9 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 6 R.T. EstCone Area Relative to ISTD RT. 30.25 1.58 ug/1 498525 Chrysene-d12 33.03 Hit# of 5 Tentatjve ID MW MolForm caAs# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 33 2 Benzoic acid, 4,4-bis[(trimethylsil 370 C16H30048i3 010586-16-0 27 3 3-IsopropoxyA1,1,1,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 10 4 Silanamine /N- [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 9 ‘Roundance ‘Sean 2745 (30.245 miny: SOBS4.D () Z 73.00 100.00 i) 1200) 147 : at A i 30.00 _30.20_30. H ry 428 x 1.40 _30.60 | Bombe inte hinge ie “tinh | m/z 147.00 36.91 ylz-> 40 60 _80_100 120 140 160 180 200 220 240 260 280 300 320 340 360 380.400 420 Abundance ? ‘#66714: 1,1,1,5,7,7,7-Heplamethy/-3,S-bis(timethyisliony}t { t 147, joo | id 355, 429. |» 30100 "30.20 ‘30140 ‘30.60 i ae 207 | | m/z 221.0 20.13 i t 4 mvz—> 40 60 _80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance ‘#73975; Benzoic acid, 2.4-bis[(trimathylsilyijoxy}-. timet if 2 | |" poo aaz0_ sola uso | 5000: 355 | m/z 355.0! 12.46 | 4s j 133 493223 281 miz> "40 60 8D 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400.420 ‘Abundance ‘#49645: 3-Isopropoxy-1,1,7,5,5,5-hexamethyl-3-(timethyisil i 281 30.00 30.20 30.40 30.60 m/z , ° 281.0) 12.39 | $000 207 339 193477 rn imiz—>____ 40-60-80 +100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 30.00 30.20 30.40 30.60 "| 30634.D. GCMS0103.M Thu Jan 10 14:10:14 2002 Page 9 NYC-WTC_000017314

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NYC-WTC_000017314Source: NYC Law Department, mirrored locally

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