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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017315
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document : Library Search Compound Report iz Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc p Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eeveeterrrrrrrerer fe rtrrrrrrrrrrttrtrrrrrrrrt titi iit rrr r irri rrr sy Peak Number 10 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7 R.T. EstCone Area Relative to ISTD R.T. 31.71 1.46 ug/l 458521 Chrysene-d12 33.03 Hit# of 5 Tentative-tp MW MolForm cas# Qual 1 3-Isopropoxy-1,1,%,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 2 2-Hexenedioic agid,.bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 3 Butanoic acid,/3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 23 4 Ethanedioic afid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 23 Rbundance ‘Scan 2006 (31.714 min): 30634.D (-) m/z 73.00 100.00% ] | | 5000: 147 \ ot 355 428 31.40 31.60 _31.80_32.00 45 197 sony | 249 325 401 Se Ue CRT Ins __"'§0” tbo. 160 260280" 9b0 980 400.” 50” 50880 pundanes 8 #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethy!-3,5,5-tris(trim i | | 147 31.40 _31.60_31.80_32.00 m/z 221.0 22.50% | 2 2Btaa7 415 519561 2 > ‘100150200 250 300 360400450600 550 Abundance - ‘#40777; 2-Hoxenediois acid, bis(trimethyisily!) ester, (E+ 31.40 _31,60_31.80 32.00 1 e000. m/z 281.0 15.03% | Bt 147 | i | | 142 244 273 | mvz->__80__100 _150_200_250__300__350__400 450 __500_550 pans #T17BZ: Butandle acid, S-methy-2-|(rimethyisiyjoxy)-,t 31.40 31.60 _31.80_32.00 | 145 m/z 355.0) 10.193 i} 5000. | “5 i I 447, 190 219 247 ini 50100 150 200 250 300 350 400450 500560 | 31.40 31.60 31.80 32.00 30634.D GCMS0103.M Thu Jan 10 14:10:21 2002 Page 10 NYC-WTC_000017315

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NYC-WTC_000017315Source: NYC Law Department, mirrored locally

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