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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017316
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NYC 9/11 Public Portal Document : Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eererererrrrrrerrr ster errrrretrrererrrtrrrtrr tt tri t rit tia titi t tris Peak Number 11 Ethanedioic acid, bis(trimethy Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.38 1.10 ug/1 v 345996 Chrysene-d12 33.03 Hit# of 5 Tenvative ID MW MolForm cas# Qual 1 Ethanedioic Acid, bis(trimethylsily 234 CeH1804si2 018294-04-7 32 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 25 3 Butanoic Acid, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 23 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576. C18H5207Si7 071579-69-6 17 Rburdance ‘Scan 5195 (34.376 min): 30634.D ¢) m/z 73.00 100.003 | | 5000. 147 \ 224 ! si we 429 | 34100 3420 3440 34.60 34.80 | Fereprh ota Then 28 wo as m/z 147.00 49.993 Mniz->__40_ 60 _80_100 120 140 160 180 200 220240 260 280 300 320 340 360 380400420 ‘Abundance ‘#71006: Ethanedioic acid, bis(trimethyisilyl) ester | | | 147 | sooo: | epee? ane ii 34,00 34.20 34.40 34.60 34.80 45 m/z 221.0, 28.39% ‘ U7, 190 219 w-> "0. 60.8 100 120 140 160 100 200 250 240 260 260 300 320 340 360 380 400 420, indance b= GSTS: 1.1,4.5.7.7, F-Heptamethy-3.3-bisthimethyisiloxy jt : 147 34.00 34.20 34.40 34.60 34.80. 5000 267 z 281.00 17.27% i 385 428 | 6 207 i | fa | if | => _" 49 6080 100 120 140 160 180 200 220 240 260 260 300 320 340 360380400 420 | undance ‘#71782: Butanoic acid, 3-methy!-2-[(trimethyisilyNoxy}-, t 34,00 34.20 34.40 34.60 34.80 | 145 m/z 355.0, 15.69% | | 6000: i | 45 reaver eopteyren ern porn pereepmnprerperrrepeeenperpe | epee as "20 "B6 eb 180120140 100 160 200250240 260260 980380340380 580400420" | 34.00 ‘34 34.00 _34.20 34.40 _34,60 34.80 30634.D GCMS0103.M Thu Jan 10 14:10:26 2002 Page 11 NYC-WTC_000017316

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NYC-WTC_000017316Source: NYC Law Department, mirrored locally

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