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GCMS analysis results for sample AD30633, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.

NYC-WTC_000017210–000017232

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017229
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Ethanedioic acid, bis(trimethy Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 34.38 0.96 ug/ 306031 Chrysene-dl2 33.03 Hit# of 5 'entative ID MW MolForm CAS# Qual l Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 32 3 1,1,1/5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 4 2-Propenoic acid, 2-[(trimethylsily 232 C9H20O3Si2 055191-13-4 23 Abundane Scan 3195 (34.378 mln): 30633.D (-) m/z 73.00 100.00% 73

147 5000 221 281 355 1 i 1 1 • • i • 34.00 34.20 34.40 34.60 34.80

m/z-> 45 nompour TMhppI 96 117 Tpmmt 251, 191 1 251 , 40 60 80 100120140160180200220240260280300320340360380400420 27 4 401 429 TTmp m/z 147.00 50.57% Abundance #71005: Ethanedioic acid, bis(trimethylsilyl) ester 73

147 5000 ■ । ■ ■ ■ ■ ।111/11 1 ■ • i •

45 m/z 7 " 39% 34.00 34.20 34.40 34.60 34.80

n/z-> +H 117 „ TprTTpTTTprrfrp- , 190 219 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5.5.5-hexamethy-3,3-bis[(trimet

“x " 73 147 34.00 34.20 34.40 34.60 34.80 5000 281 45 369 117 i 207 249 rTTJTTTTJTTTTJ" PICDT TWB1U090002—8811"T092—B8—ITa m/z-> 40 60 80 100120146160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t ■ * i‘ 73 34.00 34.20 34.40 34.60 34.80 m/z 355.0 15.64% 147 5000 267 355 429 45 207 UIU110300—0000—00033311501117 T’I .... ................. pTTTprrqTrnr Tr n T T Lr miz—> 40 60 80 100120140160180200220240260280300320340360380400420 34.00 34.20 34.40 34.60 34.80

30633.D GCMS0103.M Thu Jan 10 15:24:42 2002 Page 13

NYC-WTC_000017229

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NYC-WTC_000017229Source: NYC Law Department, mirrored locally

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