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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017207
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 . Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peeeeeererrerrrrrrrr srt rrrerrrrrrrrtrrrtrrrtrttrri titi tet irri Trt ted Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9 R.T. _EstCone Area Relative to ISTD R.T. 30.25 0.43 ug/l 124064 Chrysene-d12 33.02 Hit# of 5 Tentativ€ ID MW MolForm cas# Qual 1 3-Isopropoxy-1,4,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 2 1-Monolinolep¥iglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 3 1,1,1,5,7,/7-Heptamethyl-3,3-bis(t 444 C13H4005sié 038147-00-1 23 4 Silanaming, N-[2,6-dimethyl-4-[(tri_ 281 C14H27NOSi2 072088-09-6 22 dance, ‘Scan 2746 (80.248 min}: 30608.D (-) Zz 73.00 100.00% 000 147 7 et a5 429 30.00 _30.20 30.40 _30.60 te eh tes caeeheaetey come) m/z 147.00 35.79 Pelee gg 0.100, 150. 200200. 900.200. 400.. 450___500_ 550. (Abundance = #60503: 3 leopropaxy-1,1,1,7,7,7-hexamethy-3.5.6-tis(tim | 5000- 147 5 '30.00 30.20 30.40 30.60. \ m/z 221.0) 20.87; il 2M sar 415 519561 > 50100 150200250300 350400 450 500550 indance- 7 ‘#58671: 1-Monolinoleoyigiycero! trimethyisily| ether | 207 L 30.00 _30.20 30.40 _30.60 | sooo 147 | m/z 355.0 13.06 34 103 | 1 281 | | | - = #82 a 50. 100__150_ 200 _250 300 350 400 450 500 550. indance ‘#56714: 1,1,1,5,7,7,7-Heptamethy-3,3-bis(trimethyisiioxy)t — 30.00 30.20 30.40 30.60 | m/z 281.0, 12.70 147 | 5000. 267 355 | a 207 429 miz> 50100150200 «250-300-380 40045050050 30,00 30.20 30.40 30.60 30608.D GCMS0103.M Thu Jan 10 15:08:32 2002 Page 9 NYC-WTC_000017207

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NYC-WTC_000017207Source: NYC Law Department, mirrored locally

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