NYC 9/11 Public Portal Document
Library Search Compound Report
4 Data File : M:\INSTRU~1\209\DATA\DEC2701\30604.D Vial: 34
Acq On : 28 Dec 2001 10:13 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Misc : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Pereveetrrrrrrrrererrertrrrrtttrrrrrrtrrrtrtrrtriirrr itil ttt lt
Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2
R.T. EstCone Area Relative to ISTD R.T.
17.45 1.99 ug/l 633168 Naphthalene-d8 15.28
Hit# of 5 Tenyative ID MW MolForm cas# Qual
1 1,1,1,5,7,7,7/Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25
2 2H-1,4-Benzodgiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22
3 Silane, [1,2/3-benzenetriyltris(oxy 342 C15H3003Si3 017864-23-2 10
4 Pregnane-3,70-dione, 11-[(trimethyl 462 C26H46N203Si__057305-27-8 9
dance ‘Scan 1351 (17.449 min): 30604.D (-) m/z 73.00 100.00%
' |
| s000: |
I i |
( 45 w 429 17.20 17.40 17.60 17.80
| 447 179, 207225 251 281 311 4 397 he m/z 341.0 27.33%
jniz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 __
Abundance #56714; 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethyisiloxy}t |
| |
i} 147 |
| S000 on 255 a0 17.20 4740 17.60 17.80 _|
45 207 | m/z 147.00 13.603
= '40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400420 |
pa #49397: 2H-1 4-Benzodiazopin-2-one. 7-chioro-1.3-dihyaro-5- |
at |
|
| i L 47.20 _17.40_17.60_17.80
‘5000 i i m/z 325.00 10.19:
| a |
| ; ot
| | 846 ze eo ats,
bven> "20. 60 80 100 120 140 160 180 200 220 240 280 260 300 320 340 260 380 400.420
(Abundance #48324: Silane, [1,2,3-benzenetrlyltris(oxy)jtris|trimethyl-
j 17.20_17.40_17.60_ 17.80.
239 m/z 342.0, 9.28%
5000: 342
45
493479214 314
> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380.400 420 47.20 17.40 17.60 17.80 |
30604.D GCMS0103.M Thu Jan 10 15:04:27 2002 Page 4
NYC-WTC_000017167
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