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GCMS scan data for sample AD30604

Machine-extracted title · confidence 90%

Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.

NYC-WTC_000017157–000017170

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

Page image
Scanned page image, NYC-WTC_000017167
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report 4 Data File : M:\INSTRU~1\209\DATA\DEC2701\30604.D Vial: 34 Acq On : 28 Dec 2001 10:13 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Pereveetrrrrrrrrererrertrrrrtttrrrrrrtrrrtrtrrtriirrr itil ttt lt Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2 R.T. EstCone Area Relative to ISTD R.T. 17.45 1.99 ug/l 633168 Naphthalene-d8 15.28 Hit# of 5 Tenyative ID MW MolForm cas# Qual 1 1,1,1,5,7,7,7/Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 25 2 2H-1,4-Benzodgiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 3 Silane, [1,2/3-benzenetriyltris(oxy 342 C15H3003Si3 017864-23-2 10 4 Pregnane-3,70-dione, 11-[(trimethyl 462 C26H46N203Si__057305-27-8 9 dance ‘Scan 1351 (17.449 min): 30604.D (-) m/z 73.00 100.00% ' | | s000: | I i | ( 45 w 429 17.20 17.40 17.60 17.80 | 447 179, 207225 251 281 311 4 397 he m/z 341.0 27.33% jniz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 __ Abundance #56714; 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethyisiloxy}t | | | i} 147 | | S000 on 255 a0 17.20 4740 17.60 17.80 _| 45 207 | m/z 147.00 13.603 = '40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400420 | pa #49397: 2H-1 4-Benzodiazopin-2-one. 7-chioro-1.3-dihyaro-5- | at | | | i L 47.20 _17.40_17.60_17.80 ‘5000 i i m/z 325.00 10.19: | a | | ; ot | | 846 ze eo ats, bven> "20. 60 80 100 120 140 160 180 200 220 240 280 260 300 320 340 260 380 400.420 (Abundance #48324: Silane, [1,2,3-benzenetrlyltris(oxy)jtris|trimethyl- j 17.20_17.40_17.60_ 17.80. 239 m/z 342.0, 9.28% 5000: 342 45 493479214 314 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380.400 420 47.20 17.40 17.60 17.80 | 30604.D GCMS0103.M Thu Jan 10 15:04:27 2002 Page 4 NYC-WTC_000017167

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NYC-WTC_000017167Source: NYC Law Department, mirrored locally

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