NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\26827.D Vial: 11
Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS- Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 7 Cyclohexasiloxane, dodecamethy Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
17.45 0.32 ug/1 128652 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW Mol Form CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36
2 1,1,1,5,7,7,7-Hpptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25
3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N2OS1 055299-24-6 12
4 Silane, [1,2 -benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 10
Abundance / Scan 1352 (17.453 min): 26827.D (-) m/z 73.00 100.00%
73
5000
341
147
m/z->
m45 117 . 1
TDTmma
179.. 207 251 295 [ 1
TfTu OadU-rrT j »i q nn pm jim 11
40 60 80 100120140160180200220240260280300320340360380400420
429
mmh m/z 341.0,0
17.20 17.40 17.60 17.80
30.33%
Abundance #56711: Cyclohexasiloxane, dodecamethyl-
73
341
429 ....................
5000
17.20 17.40 17.60 17.80
147 m/z 147.00 13.51%
miz->
... | . 117. |.. 207 .. . 311.
40 60 80 100120140 160 180 200 220240 260 280 300 320 340 360 380 400420
L
1115"
Abundance: #58714:1.1,1,5,7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t
73
T T T ITT
147 17.20 17.40 17.60 17.80
5000 267 m/z 324.90 10.49%
355 429
45 207 । 1
I ll | ' '
mpmmmpmmppmmmtmmmmmmm
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #48337:2H-1,4-Benzodlazepin-2-one, 7-chloro-1,3-dihydro-5- l *4* J » » l’« 11 I I I it < I I I " I 1
73 341 17.20 17.40 17.60 17.80
m/z 342.0,0 10.09%
5000
45
91
..
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 " 17.20 17.40 17.60 17.80
26827.D GCMS1126.M Tue Jan 29 14:25:12 2002 Page 7
NYC-WTC_000018911
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