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GCMS analysis log for sample AD30603

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.

NYC-WTC_000017233–000017245

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017242
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NYC 9/11 Public Portal Document Library Search Compound Report rE Data File : M:\INSTRU~1\209\DATA\DEC2701\30603.D Vial: 31 Acq On : 28 Dec 2001 7:17 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc 7 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method. : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IIIS IIE IEE ISI ISIS IIS IIIS IOI ISO IIS IIS IIE I IOI IO IIIS I IOI IE Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. | EstConc Area Relative to ISTD R.T. 17.45 1.22 ug/l 618419 Naphthalene-ds 15.28 . Hit# of 5 Téntative ID MW MolForm cas# Qual 1 Cyclohexasifoxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 59 2 2H-1,4-BenZodiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 3 Silane, JA,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 12 4 1,1,1,5,//,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 __038147-00-1 12 ‘Scan 1352 (17.454 min}: 30603.D (-) m/z 73.00 ey - | at i 45 “7 uid 179. 207295 251 281 311 sor “7? ~ "4720 “174047160 _ 17.80 m/z 341.00 32.71% z—>__40 60 _80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 Ras #56711: Cyclohexasiloxane, dodecamethy!- ut | 429 _ 17.20 4740_ 17.60 17.80 i 147 m/z 147.00 14.26' | 117 207 ae > AO _60_80 100 120 140 160 180200 220 240 260 280 300 320 340 360 380 400420 indance ‘#BA8337; 2H-1,4-Benzodiezepin-2-one, 7-chioro-1,3-dihydro-5- 73 ut 17.20 17.40 17.60 _17.80__| 5000: i m/z 324.90 11.21% | 45 { 1 | 116 146 227 269 gas > 40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 ‘ ibundance “#48324: Silane, [1,2,3-benzenetrlyltris(oxy)]tris[trimethyl- 17.20 _17.40_17.60_17.80 | a [m/z 342.00 10.77% | 5000: | a2 45 | | 193479214 314 fniz—>_40_60_80_ 100120 140 160 180 200220240 200 280 300320 340 360 380400420 __ 17.20_17.40_17.60_17.80 30603.D GCMS0103.M Thu Jan 10 15:01:42 2002 Page 3 NYC-WTC_000017242 :

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NYC-WTC_000017242Source: NYC Law Department, mirrored locally

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