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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D vial: 24 Acq On : 9 Jan 2002 12:45 pm Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS ISOS ISIS SISOS III ISI IOI I IOI ISI ISI IOI TI TATOO TOI IOI IOI TAI OI IATA Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstConc Area Relative to ISTD RT. 17.31 2.47 ug/l 889180 Naphthalene-d8 15.12 Hit# of 5 Tentgive ID MW MolForm cas#t Qual 1 Cyclohexasiloyéne, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 2H-1,4-Benzgdiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 3 1,1,1,5,7,%,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 12 _4 Silane, ,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 10 (Abundance ‘Scan 1336 (17.308 min}: 31019.D () [* Z 73.00 100.00% | | | mn | | 45 96 117 v 479, 207295 251 261 311 307 ad {1.00 _17:20_1740_17.80 | : = A m/z 341.00 32.47 iptac 40_60_ 80 100 120 140 160 180 200 220 240 260-280 300 320 340 360 380 400420 indance #86711: Cycichexasiloxane, dodecamethy!- | 34t ~ | _ — if 47.00 _17.20_17.40_ 17.60 | 147 m/z 147.00 15.47% = 47, 207 267 314 = 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400420 Rie eee SE BAI adenzodiazepi-2-one, Fchioro-t,S-diiydros 1 RB at j | 17.00 _17.20 17.40 17.60 5000: m/z 325.00 11.49% 6 1 : 116 146 27 280s “Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-dis(trimethyisiloxy)t | 17.00 17.20 17.40_ 17.60 i m/z 342.00 10.85% | 147 | 8000: 267 | aad 429 | 45 | 207 | iniz-> "4060. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 360 400 420 171001720 4740 17.60. 31019.D GCMS0103.M Thu Jan 10 16:01:26 2002 Page 3 NYC-WTC_000017564

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NYC-WTC_000017564Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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