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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017563
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 dan 2002 12:45 pm Operator: 209 GALOS sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Pereronrrer er rer rer rrerrrrrrrrrrrrrrrrrtrr rr or littl tri Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. | EstCone Area Relative to ISTD R.T. 14.17 1.40 ug/l 503754 Naphthalene-ds 15.12 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Cyclopentagfloxane, decamethyl- 370 C10H3005Si5 000541-02-6 56 2 N-(Triflyéroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 3,4-Diby@roxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzepéethanamine, N-[(pentafluorop 475 C21H26F5NO2Si2_055429-85-1 38 Rbundance ‘Scan 904 (14.168 min}: 1079. © m/z 73.00 100.008 | S000: 287 | 355 45 493 43.80 14.00 14.20 14.40 | 103133154 (223 293 323 m/z 267.00 36.02! oes. 50100 150200 2803003504008 i indance #61266: Cyclopentasiioxane, decamethyl- | f s i} 355 | 267 bed | | 43.80 14.00 14.20 14.40 | | m/z 355.0; 25.58) i i 207 323 bz 50100 150 «200250 300350400450 (Abundance 58326, NET Afluoroacety!)-G.0" 0" -trisirimethyisilyline: i 3 i i bi 13.80 14.00 14.20 14.40 | s000: m/z 268.00 9.55% ! i 45 | | is 126147 __ 193 265 376 481 | Ine> __" 90100160 __200_250___300___ 360400450. | Abundance #49868: 3 A-Dihydroxybenzyl alcohol tis (timethyisliyl> — ' 43.80 14,00 14,20 14.40 ? m/z 356.0, 9,254 i : | S000: | 170 Cd | 45 | 147 ° | | 209 237 312 mz—> 50 100150 ~=— 200s 250 300 380400 450] 13.80 14.00 14.20 14.40 31019.D GCMS0103.M Thu Jan 10 16:01:20 2002 Page 2 NYC-WTC_000017563

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NYC-WTC_000017563Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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