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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017201
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NYC 9/11 Public Portal Document : Library Search Compound Report : Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K. L Perrrrrrrririre titer terre rr tere rer Iti trrt tt rt tt rert rere t eters Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstCone Area Relative to ISTD R.T. 14.31 1.31 ug/1 518333 Naphthalene-ds 15.28 Hit# of 5 Tentative MW MolForm cAS# Qual 1 Cyclopentasiloxane /decamethyl- 370 C10H3005Si5 000541-02-6 72 2 3,4-Dihydroxyben: alcohol, tris(tr 356 C16H3203Si3 068595-79-9 38 3 N-(Trifluoroacef¥1)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Benzoic acid, 2%,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 37 (Abundance ‘Scan 1009 (14.310 min}: 30608.D (-) m/z 73.00 100.008 15000: | | "ss —_ 45 193 44.00 14.20 14.40 14.60 oom te slee | m/z 267.00 37.42 mz __50___100___ 4 200 _250__300_350__400 _ 450 ‘Abundances o #51286: Cydopentaslioxane, decamethyr | | 355 | Pe | 5000: L 14.00 14.20 14.40 14.60 m/z 355.0 30.50 1 207 323 eee 50100 150 «200-250 3003504005. indance 73 HRBBE: SADinyerorjDonzyaloonol eistmotaly- ‘14.00 14.20 14.40 14.60 15000: 178 ei m/z 356.0, 11.29 t 358 | 45 147 ao _ 209 237 312, a a a a oe eee indance ‘#58326: N-(Trifluoroacety!)}-0,07,0*-tris(trimethyisiiyjno 14.00 14.20 14.40 14.60 ae m/z 267.90 10.23 | 5000. | i 6 126147 193 265 376 481 feo "We 80” Bos Bo aslo | doa 14.40 14.60 30608.D GCMS0103.M Thu Jan 10 15:08:01 2002 Page 3 NYC-WTC_000017201

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NYC-WTC_000017201Source: NYC Law Department, mirrored locally

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