NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis results for sample AD28860, Dec 16 2001
Machine-extracted title · confidence 100%Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
NYC-WTC_000018817–000018829Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\29735.D Vial: 18 Acq On : 29 Dec 2001 3:45 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.30 0.66 ug/1 257801 Naphthalene-d8 15.28
Hit# of 5 entative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 47 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46 4 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1009 (14.304 mln): 29735.D (-) m/z 72.95 100.00% 73
5000 267 355
mte~> m 45 , 89 108 133 154 177 193 . 223 323339 } IImIuumomum—auagTamT 1’1—2011—00103 251 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60 m/z 267.00 32.46% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 T i 1 Pi T-r-j-r-r 14.00 14.20 1440 1460 m/z 355.0 21.47% ................... ;................. '191207....... 2514....................... 323339 ..... m/z-> 40 60 80 100 120 140 160 180 '266 220 240 260 280 300 320 340 360 ‘ Abundance #<3978: Benzoic acid, 2.5-bis(trimethylsiloxy)-, trimethyls 73 355 T T ' I ‘ ‘ ‘ ‘ I ' ' 14.00 14,20 14.40 14.60 5000 m/z 9.97% 45 1... .147179207223, ................. . m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ’ Abundance #49868:3.4-Dihydroxybenzyl alcohol, tris(trimethylsily)- T-r-p-r • 1 • 4 73 14.00 14.20 14.40 14.60 m/z 356.05 8.96% 5000 267 179 356
m/z~> 45 147
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ' 312 341 m14.00 14.20 14.40 14.60
29735.D GCMS1126.M Tue Jan 29 14:27:17 2002 Page 3
NYC-WTC_000018826
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NYC-WTC_000018826Source: NYC Law Department, mirrored locally
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