GCMS results for unknowns, sample AD30488, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC2701\30488.D Vial: 16 Acq On : 29 Dec 2001 1:48 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 1.13 ug/1 480400 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxa , decamethyl- 370 C10H3005Si5 000541-02-6 39 2 N- (Trifluoracety1)-0,0’,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 3 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 Benzeneaceti acid, .alpha.,4-bis[( 326 C15H26O4Si2 055334-40-2 37 Abundance.............. ’ Scan 1009 (14.308 min): 30488.D (-) m/z 73.0,0 100.00% 73

5000 267 355 i rp ■ i 1 ‘ • i 1 1 ' • i 45 193 223 14.00 14.20 14.40 14.60 — 108 133154 ,T 293 323 k **1***1*’+}+ m/z 267.00 32.28% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 ‘ ‘ ‘ m/z 355.0 24.85% 207 323 • ■ i ■ ‘ ‘ ■ i 1 ■ ■ “ i ■ • ■ • i • ■ ' ■ I 1 1 ■ i ' ■ • i ■ ■ ■ • i ■ • 1 ■ i 1 ■ ■ • i 1 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58807; N-CTnfluoracetyD-O.O'.O'-tristtrimethylsilyljepin 73 355 TCTCTESITT/BI/O/5/0/01/S/5..I 14.00 14.20 14.40 14.60 5000 m/z 267.9.0 9.12%

45 ! h 140 184 281 480 1 1 1 1 11 * 1 * • i t | | l < > | i i > < | r i I i । t i i > | i » I i | i i'l l 1'1' i r t "i ‘i miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #74573: Benzeneethanamine, N-[(pentafluoropheny!)methylene] 73 14.00 14.20 14.40 14.60 m/z 356.0 8.95% 5000 267 44 _ I , M.............. 151 179 209 237 [...................................................... miz~> 50 100 150 200 250 300 350 ‘400 450 ‘500 14.00 14.20 14.40 14.60

30488.D GCMS1126.M Tue Jan 29 14:30:24 2002 Page 4

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