NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~l\209\DATA\DEC2701\LBB.D Vial: 24
Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
14.30 0.47 ug/1 216772 Naphthalene-d8 15.29
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72
2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46
3 Benzoic id, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 43
4 Benzene^ hanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37
Abundance Scan 1009 (14.304 mln): LBB.D (-) m/z 73.00 1 00.00%
| 73
5000
267 ,, i j t i — ] 4 , | rr । » ] i i'i' r-
355
Mz~>
m 45
k 103
TTT
133 154 177 193
i-| n n । n mrsfumn |T mppmpmpmmm
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
223 251 , $2333
3233 9
‘I
14.00 14.20 14.40 14.60
m/z 267.00 31.81%
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
.................... /...................
355
267
5000
14.00 14.20 14.40 14.60
m/z 355.0 23.07%
191207 251 323339 J
*‘X—2—21921*‘***1/**/1****I Puana I• •i I “ ’ 41 TPWP T
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
•Abundance #40868: 3,4-Dihydroxybenzy! alcohol, tris(trimethylsilyl)-
73
267
14.00 14.20 14.40 14.60
5000 179 m/z 267.90 9.24%
356
45 147
209 237 312 341
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #73978: Benzoic acid, 2,5-bis(trimethylslloxy)-, trimethyls
73 14.00 14.20 1440 14.60
355 m/z 356.0 9.12%
5000
45
I , 147 179 207223 _ 267282297 I 370
. ! | I k I • J » J l' | I, I .»I! ..»I H . . J . T I I | I I . » | » . . i J . I I I J I I . . | . I | r» i I |
. I fj . ! TLWDIII T T
m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
LBB.D GCMS0103.M Thu Jan 10 13:58:35 2002 Page 2
NYC-WTC_000017133
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