Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
NYC-WTC_000017144–000017156Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30601.D Vial: 29 Acq On : 28 Dec 2001 5:20 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 14.30 0.72 ug/1 352476 Naphthalene-d8 15.29
Hit# of 5 entative ID MW MolForm CAS# Qual 1 Cyclopenta: loxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Benzoic ac d, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46 4 Benzoic cid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 Abundance 73 Scan 1009 (14.304 mln): 30601.D (-) m/z 73.0,0 100.00%
5000 267 355 45 45 t , 89 108 133 154 177 193 223 251 . 323339 i 14.00 14.20 14.40 14.60 ‘ ■ ■ ‘ I'■' ‘11 MTt n 177 fm FIriy 11 hpeei rri r’rrurp I *TIpnugnu —uaT m/z 267.00 32.38% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 5000 267 ..... J y.. 14.00 14.20 14.40 14.60 m/z 355.0 23.23% ____ 191207 251 . 323339 ।।।(।।, •> 1111111111 > 11 111111111 1111 j'i i n'| 11 i •»• • i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bis(trimethylsiloxy)-, trimethyls 78 355 ________________ _____ • ■ i ■ ■ • ■ i ■ ■ ■ ■ i ‘ 1 • ■ i ■ • 14.00 14.20 14.40 14.60 5000 m/z 74.00 8.33% 45 1....... 147 _, 179 ,, 207223 . .. 267282 370 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 73 #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- ... 1... 1 ‘ I ' ‘ ‘ I ‘ ‘ • I ‘ 1 1 1 I 1 1 14.00 14.20 14.40 14.60 m/z 356.0 8.20% 5000 267 179 356 45 147 I , I, । 209 237 i i i j A i < । l t i i । i > i i । t i i : । i i H j «Vi i । i < i i i > i i । i > । । । , 312 341 । । | । । Y । । > 7 i i । t i > > । i i < ( । i f I J J* t 1 l r|"T T l' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30601.D GCMS0103.M Thu Jan 10 14:05:18 2002 Page 2
NYC-WTC_000017152
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NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017233
Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018923
GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018858
GCMS analysis report for sample AD30606 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017157
Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018870
GCMS analysis report for sample AD30485 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017770
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036931
GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder