Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
NYC-WTC_000017144–000017156Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\30601.D ; Vial: 29 Acq On : 28 Dec 2001 5:20 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
7.61 4.20 ug/1 1643670 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 1-Butanamine, 3-methyl - 87 C5H13N 000107-85-7 7 Abundance Scan 280 (7.611 min): 30601 .D (-) m/z 73.00 100.00% 73
5000 43 T' ' 1 1 I 1 1 I 1 ITITi 1 I ■ ■ 7.20 7.40 7.60 7.80 8.00 0- ........ 38.1 149 T 55, 60 67, । + 87 103 • • i ■ ■ • • i • ' ■ • i ■ • 1 1 r1 1 1 1 1 1 7 | ' i I j T~~l I J | it I 1J I n m/ z 43.0,0 31.61% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73
5000 1 1 14 t a 1" 'I 1 1 1 1 11TT 44 58 7.20 7.40 7.60 7.80 8.00 I m/z 45.0,5 11.51% 15 -P— i i • * ■ 4 t * 1 '* * j * ‘ • t * > • < i ' * i * I * i * • । ■ mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845; Silane, tetramethyl- 73 pI » » Tanl । j j i ri 1 in’ i i ।'! R 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 11.39%
45 15 31 55 , 88 1 • i ■ ‘ ■ 1 1 1 1 1 1 r1 1 t J | t i j i । i i11 ‘ r1 j i n j । F • ■ ■ i ■ ■ • 1 i ■ • 1 1 i 1 1 1 1 r1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.85% 5000 45
1 i ‘ 27 33 39 , 55 ■ i • • ■ • i * ‘ ‘ 1 । i . . T1 » j » < j » i 4 I t —mom m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 ' 7.40 ' 7.60 ' 7.80 8.00 '
30601.D GCMS0103.M Thu Jan 10 14:05:12 2002 Page 1
NYC-WTC_000017151
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NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017233
Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018923
GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018858
GCMS analysis report for sample AD30606 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017157
Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018870
GCMS analysis report for sample AD30485 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017782
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD303B5 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017770
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036931
GCMS analysis report for sample AD29565 listing unknown compounds and surrogate recovery data from January 22, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder